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Citation: JIANG Xiao-Ying, GU Yong-Qing, LI Xiao-Bo, LI Jian-Ping. Synthesis and Characterization of N,N'-Diary Adipyl Bis-azo Compounds[J]. Chinese Journal of Applied Chemistry, ;2008, 25(6): 747-749. shu

Synthesis and Characterization of N,N'-Diary Adipyl Bis-azo Compounds

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a Henan Institue of Science and Technology, Xinxiang 453003;
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b College of Chemistry & Enviromental Science, Henan Normal University, Xinxiang

Corresponding author: JIANG Xiao-Ying,
Received Date: 18 June 2007
Available Online: 8 September 2007
Fund Project: 河南省自然科学基金资助项目(0111010680) (0111010680)

A series of N,N'-diary adipyl bis-azo compounds was synthesized from home-made N,N'-diaryl adipyl dihydrazide via oxidation system Fe(NO₃)₃·9H₂O.The products were confirmed by elemental analysis,IR and ¹H NMR.Two N-H absorption peaks of N,N'-diaryl adipyl dihydrazide in the infrared spectrum were approximately at 3 200~3 400 cm^-1,while the two N-H absorption peaks were disappeared for oxidized products;two N-H chemical shifts of N,N'-diaryl adipyl dihydrazide in ¹H NMR were about from 7.3 to 10.5,however,the same N-H chemical shifts were missing oxidized products;the results of elemental analyses for the products are in accord with their theoretical values.The yields were about from 80% to 94%.
- N,N'-diaryl adipyl dihydrazide,
- N,N'-diary adipyl bis-azo compound,
- synthesis
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