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Citation: HUANG Bao-Mei, YAO Cheng-Wei, WANG Xiu-Feng, WANG Zhi-Guo, MI Jin-Yuan. Determination of Furazolidone Residue in Shrimp by Capillary Electrophoresis with Amperometric Detection[J]. Chinese Journal of Applied Chemistry, ;2008, 25(6): 730-733. shu

Determination of Furazolidone Residue in Shrimp by Capillary Electrophoresis with Amperometric Detection

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a Chemical Department of MianYang Normal University, Mianyang 621000;
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b The 4th Institute of CARDC, Mianyang;
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c School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou

Corresponding author: HUANG Bao-Mei,
Received Date: 9 July 2007
Available Online: 6 September 2007

A method for the determination of furazolidone residue in shrimp by high performance capillary electrophoresis with amperometric detection system was established.Several parameters affecting the determination were studied,including running buffer concentration,acidity,sampling time and separation voltage and organic additive.Under the following conditions:Na₂B₄O₇-NaOH(Na₂B₄O₇ 30 mmol/L,pH=9.0 as buffer solution,CH₃OH as organic additive,25 kV as running voltage,a linearity exists between peak height (Y) and mass concentration (c) in a range of 0.5~100 mg/L,the linear coefficient is 0.999 2,determination limit is 0.01 mg/L.
- capillary electrophoresis,
- furazolidone,
- amperometric detection
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