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Citation: WAN Li-Juan, FU Hong-Gang, SHI Ke-Ying. “Flower-like”Nanocrystalline CdS Electrodeposited on SBA-16 Thin Film/ITO Substrate[J]. Chinese Journal of Applied Chemistry, ;2008, 25(7): 759-762. shu

“Flower-like”Nanocrystalline CdS Electrodeposited on SBA-16 Thin Film/ITO Substrate

WAN Li-Juan ^a,b ,
FU Hong-Gang ^a,b,, ,
SHI Ke-Ying ^b

1.
a Department of Applied Chemistry, Harbin Institute of Technology, Harbin 150001;
2.
b Laboratory of Physical Chemistry, School of Chemistry and Materials Science, Heilongjiang University, Harbin

Corresponding author: FU Hong-Gang,
Received Date: 26 July 2007
Available Online: 23 September 2007
Fund Project: 国家自然科学基金重点(20431030) (20431030)国家自然科学基金(20671032和20676027)资助项目 (20671032和20676027)

The mesoporous SBA-16 thin films were synthesized with ITO as the substrate under acidic condition.The prepared SBA-16 thin films with narrow pore size distribution have a body-centered cubic structure (Im3m space group).In recent years,ITO-coated glass or AAO has been used as the substrates for the electrodeposition of CdS,while work on using mesoporous molecular sieves films/ITO as the substrate has not appeared.In an electrolyte solution composed of CdCl₂ and Na₂S₂O₃ with a modulated pH value of 2~3, "flower-like" nanocrystalline CdS was electrodeposited on the surface of SBA-16 thin films/ITO electrode via the DC electrodeposition method at a constant potential of -0.7 V for 50 min.The morphology and structure of the products were characterized by SEM,TEM and the PL properties were tested.The results show that the nanocrystalline CdS was grown on the surface of the electrode and not in the mesopores and showed PL properties.
- mesoporous,
- SBA-16 thin film,
- electrodeposition,
- CdS
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