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Citation: ZHANG Guang-Ju, LI Guang-Hao, HAI Hua. Simultaneous Determination of Triazinine Herbicides in Vegetable[J]. Chinese Journal of Applied Chemistry, ;2008, 25(8): 957-960. shu

Simultaneous Determination of Triazinine Herbicides in Vegetable

1.
a School of Environmental and Biological Science and Technology, Dalian University of Technology, Dalian 116023;
2.
b College of Life Science, Dalian Nationalities College, Dalian 116600

Corresponding author: LI Guang-Hao,
Received Date: 16 August 2007
Available Online: 18 November 2007

A high performance liquid chromatography(HPLC) method has been developed for the simul-taneous determination of residues of eleven triazine herbicides in vegetable. Triazine herbicides were extracted from vegetable with water/methanol and cleaned up with solid-phase extraction cartridges. Then triazine herbicides extracted were analyzed by HPLC with ultraviolet and mass spectrometric detection. The pre-treatment method of sample and chromatographic conditions of analysis were critically examined in this work. The linear ranges for the 11 triazine herbicides were 0.02×10^-6~1.0×10^-6 g/mL, with correlation coefficients of 0.998 7~0.999 9. The average recoveries for the eleven triazine herbicides in spiked vegetable were in the range of 72.1% to 101.0%, and the relative standard deviations were between 1.2% and 5.1%. The method developed is easy and fast, and has a better purification effect. It can meet the requirement for simultaneous determination of many herbicides in vegetable.
- Triazine herbicide,
- solid-phase extraction,
- tomato,
- high performance liquid chromatography
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