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Citation: KONG Ting-ting, DONG Yi-fan, ZHANG Ying-ping, ZHANG Ya-gang, ZHOU An-ning. Preparation of hydrotalcite-like Ti/Li/Al-LDHs and its performance in CO2 adsorption[J]. Journal of Fuel Chemistry and Technology, ;2016, 44(08): 1017-1024. shu

Preparation of hydrotalcite-like Ti/Li/Al-LDHs and its performance in CO2 adsorption

  • 1.

    College of Chemistry and Chemical Engineering, Xi'an University of Science and Technology, Xi'an 710054, China

  • Corresponding author: ZHOU An-ning, 
  • Received Date: 7 April 2016
    Available Online: 18 June 2016

    Fund Project:

  • A series of hydrotalcite-like Ti/Li/Al-LDHs materials were prepared by co-precipitation method and characterized by atomic absorption spectrophotometer (AAS), X-ray diffraction (XRD), scanning electron microscopy (SEM), thermal gravimetric analysis (TG) and Fourier transform infrared (FT-IR); the influence of metal composition and calcination temperature on the structure, morphology and CO2 adsorption capacity of Ti/Li/Al-LDHs was investigated. The results showed that Ti1Li3Al4-LDHs obtained with a Ti/Li/Al ratio of 1:3:4 displays the highest crystallinity and regular morphology, whereas Ti1Li3Al2-LDHs300 prepared with a Ti/Li/Al ratio of 1:3:2 and calcined at 300℃ exhibits the best adsorption performance towards CO2. The CO2 adsorption capacity over Ti1Li3Al2-LDHs300 reaches 53.5mg/g; in addition, the adsorption capacity is only decreased by 2.4% after adsorption for 10 cycles.
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