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Citation: LI Xiangqing, KANG Shizhao, TANG Yunqiu, LI Guodong, MU Jin. Preparation and Visible Light Photocatalytic Activity of Carbon Doped Titanium Dioxide Nanotubes[J]. Chinese Journal of Applied Chemistry, ;2013, 30(2): 178-184. doi: DOI:10.3724/SP.J.1095.2013.20163 shu

Preparation and Visible Light Photocatalytic Activity of Carbon Doped Titanium Dioxide Nanotubes

1.
a School of Chemical and Environmental Engineering, Shanghai Institute of Technology, Shanghai 201418, China;
2.
b State Key Laboratory of Inorganic Synthesis Preparative Chemistry, Jilin University, Changchun 130012, China

Corresponding author: MU Jin,
Received Date: 19 April 2012
Available Online: 14 May 2012
Fund Project: 国家高技术研究发展计划(2009AA05Z101) (2009AA05Z101)

Urea was used as a precursor of carbon to prepare carbon doped TiO₂ nanotubes.The products obtained were characterized with Brunauer-Emmett-Teller surface area measurement(BET),X-ray diffraction(XRD),transmission electron microscopy(TEM),energy dispersive X-ray fluoresence spectroscopy(EDX),X-ray photoelectron spectroscopy(XPS),solid diffuse reflection UV-Vis spectroscopy(DRS) and fluorescence spectroscopy.The results showed that the visible light photocatalytic activity of the TiO₂ nanotubes was improved obviously after doping C.In addition,the influences of doping amount of C,calcination temperature,dosage of catalyst and pH on the photocatalytic degradation activity of the TiO₂ nanotubes were investigated.The degradation efficiency of rodamine B could reach 91% under 3 h visible light irradiation when the amount of doping C was 5.3%,calcination temperature was 400℃,dosage of catalyst was 1.5 g/L,pH of solution was 5.
- TiO₂ nanotubes,
- carbon doping,
- preparation,
- visible light photocatalysis
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