Citation: Jiaxing Cai, Wendi Xu, Haoqiang Chi, Qian Liu, Wa Gao, Li Shi, Jingxiang Low, Zhigang Zou, Yong Zhou. Highly Efficient InOOH/ZnIn₂S₄ Hollow Sphere S-Scheme Heterojunction with 0D/2D Interface for Enhancing Photocatalytic CO₂ Conversion[J]. Acta Physico-Chimica Sinica, ;2024, 40(11): 240700. doi: 10.3866/PKU.WHXB202407002 shu

Highly Efficient InOOH/ZnIn₂S₄ Hollow Sphere S-Scheme Heterojunction with 0D/2D Interface for Enhancing Photocatalytic CO₂ Conversion

Jiaxing Cai ^{1, †} ,
Wendi Xu ^{3, †} ,
Haoqiang Chi ⁴ ,
Qian Liu ¹ ,
Wa Gao ^1,, ,
Li Shi ^3,, ,
Jingxiang Low ^{1, 5,,} ,
Zhigang Zou ⁴ ,
Yong Zhou ^{2, 4,,}

1.
School of Physical Science and Technology, Tiangong University, Tianjin 300387, China
2.
School of Chemical and Environmental Engineering, Anhui Polytechnic University, Wuhu 241000, Anhui Province, China
3.
State Key Laboratory of Organic Electronics and Information Displays & Institute of Advanced Materials (IAM), Nanjing University of Posts and Telecommunications, Nanjing 210023, China
4.
School of Physics, Jiangsu Key Laboratory of Nanotechnology, Eco-materials and Renewable Energy Research Center (ERERC), National Laboratory of Solid State Microstructures, Collaborative Innovation Center of Advanced Microstructures, Nanjing University, Nanjing 210093, China
5.
Multidisciplinary Platform of Advanced Engineering, Chemical Engineering Discipline, School of Engineering, Monash University Malaysia, Bandar Sunway 47500, Selangor, Malaysia

Corresponding author: Wa Gao, gaowa@tiangong.edu.cn Li Shi, iamlshi@njupt.edu.cn Jingxiang Low, jxlow@tiangong.edu.cn Yong Zhou, zhouyong1999@nju.edu.cn

^†

Received Date: 2 July 2024
Revised Date: 5 August 2024
Accepted Date: 5 August 2024
Available Online: 14 August 2024
Fund Project: the National Key R & D Program of China 2022YFE0126500the National Key R & D Program of China 2018YFE0208500the National Natural Science Foundation of China 21972065the National Natural Science Foundation of China 22203046the National Natural Science Foundation of China 22202152the Natural Science Foundation of Jiangsu Province BK20220006the Hefei National Laboratory for Physical Sciences at the Microscale KF2020006the Program for Guangdong Introducing Innovative and Entrepreneurial Team 2019ZL08L101the Chinese University Development Fund UDF01001159the Project of State Key Laboratory of Organic Electronics and Information Displays, Nanjing University of Posts and Telecommunications GZR2023010003Natural Science Research Start-up Foundation of Recruiting Talents of Nanjing University of Posts and Telecommunications NY221128

S-scheme heterojunction system represents a highly efficient strategy for photocatalytic applications as it can simultaneously facilitate photogenerated charge carrier separation and enhance the reduction-oxidation potentials of the photocatalyst. Despite its gigantic potential, the photocatalytic CO₂ conversion efficiency of the S-scheme heterojunction remains limited mainly attributed to the sluggish interfacial charge carrier migration and poor light utilization efficiency. Herein, we prepare an InOOH/ZnIn₂S₄ hollow sphere S-scheme heterojunction with 0D/2D contact interface for enhancing photocatalytic CO₂ conversion performance. Specifically, the hollow sphere morphology can cause the multireflection of incident light within the photocatalyst leading to enhanced light absorption of the photocatalyst. In addition, the 0D/2D contact interface can facilitate the photogenerated charge carrier migration transfer over the InOOH/ZnIn₂S₄ S-scheme heterojunction. Furthermore, combining in situ irradiated X-ray photoelectron spectroscopy (ISI-XPS) characterization and radicals trapping test, it is affirmed the accumulation of photogenerated holes and electrons respectively on InOOH and ZnIn₂S₄, which is beneficial for the effective utilization of photogenerated charge carriers. As a result, the photocatalytic CO₂ conversion performance of the optimized InOOH/ZnIn₂S₄ is ca. 25.8 times higher than that of pristine ZnIn₂S₄. Our reported results demonstrate a facile yet effective strategy for enhancing the interfacial photogenerated charge carrier migration and light utilization efficiency of S-scheme heterojunction.
- Photocatalytic CO₂ conversion,
- S-scheme heterojunction,
- ZnIn₂S₄,
- Hollow sphere,
- Contact interface
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Highly Efficient InOOH/ZnIn2S4 Hollow Sphere S-Scheme Heterojunction with 0D/2D Interface for Enhancing Photocatalytic CO2 Conversion

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通讯作者: 陈斌, bchen63@163.com

Highly Efficient InOOH/ZnIn₂S₄ Hollow Sphere S-Scheme Heterojunction with 0D/2D Interface for Enhancing Photocatalytic CO₂ Conversion