Citation:
LI Li-Ying, SONG Wen-Hua, CHEN Tie-Hong. Synthesis of Hydroxyapatite Nanoplates by the Hydrothermal Reaction Method with Anionic Amino Acid Surfactant[J]. Acta Physico-Chimica Sinica,
;2009, 25(11): 2404-2408.
doi:
10.3866/PKU.WHXB20091020
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By hydrothermal reaction method with the control of anionic amino acid surfactant N-lauroylsarcosine sodium (Sar-Na), single crystal hydroxyapatite (HAP) nanoplates were synthesized and different synthetic conditions were carefully studied. The products were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared (FTIR) spectroscopy. Results showed that hydroxyapatite nanocrystals with lengths of 0.5-1.0 μm, a width of 30 nm, and a high aspect ratio (20:1) were obtained. By increasing the concentration of N-lauroylsarcosine sodium, the morphology of the hydroxyapatite varied from oval to plate-like. These results show that N-lauroylsarcosine sodium can induce the formation of hydroxyapatite with different morphologies. The current work provides a new approach to tune the aspect ratio of hydroxyapatite nanoplates.
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Keywords:
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Hydroxyapatite
, - Nanoplate,
- N-lauroylsarcosine sodium,
- Morphology,
- Aspect ratio
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