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Citation: ZHU Lu-Ping, HUANG Wen-Ya, MA Li-Li, FU Shao-Yun, YU Ying, JIA Zhi-Jie. Synthesis and Characteristics of ZnO-CNTs Nanocomposites[J]. Acta Physico-Chimica Sinica, ;2006, 22(10): 1175-1180. doi: 10.3866/PKU.WHXB20061001 shu

Synthesis and Characteristics of ZnO-CNTs Nanocomposites

1.
Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; Graduate School of the Chinese Academy of Sciences, Beijing 100049, P. R. China; Wuhan Yaohua Pilkington Safety Glass Co. Ltd., Wuhan 430010, P. R. China; Institute of Nano-Science and Technology, Central China Normal University, Wuhan 430079, P. R. China

Received Date: 22 March 2006
Available Online: 11 October 2006

ZnO-CNTs nanocomposites were successfully synthesized by sol method using Zn(CH3COO)2•2H2O and treated multiwalled carbon nanotubes (CNTs) as raw materials and diethyleneglycol (DEG) as regent. The samples were determined by means of X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), infrared (IR) absorbence, and photoluminescence (PL) spectrum. TEM and SEM images indicated that the coating layer was composed of ZnO nanoparticles with size less than 25 nm. The effects of various experimental conditions, such as reaction duration and reaction temperature on the obtained composites were investigated as well. Finally, PL function and possible formation mechanism of ZnO-CNTs nanocomposites were proposed. The PL spectra of ZnO-CNTs nanocomposites showed obvious blue-shifts compared with that of pure ZnO nanomaterial.
- Sol method;ZnO-CNTs;Nanocomposite;IR absorbence;PL spectrum
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沈阳化工大学材料科学与工程学院沈阳 110142

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