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Citation: Song Chun-Min, Yan Zi-Feng, Max Lu. Synthesis and Characterization of Supersurface MCM-41 Zeolites[J]. Acta Physico-Chimica Sinica, ;2002, 18(03): 279-283. doi: 10.3866/PKU.WHXB20020319 shu

Synthesis and Characterization of Supersurface MCM-41 Zeolites

1.
State Key Laboratory for Heavy Oil Processing, University of Petroleum,Dongying　257061;NanoMac Ceter, Department of Chemical Engineering, The University of Queensland, Brisbane　4072 Australia

Received Date: 30 July 2001
Available Online: 15 March 2002

The mesoporous MCM41 molecular sieves with superhigh surface areas were hydrothermally synthesized by means of a novel surfactant. XRD, nitrogen adsorption,SEM and pyridine TGDTA were used to characterize the crystallinity,surface area and mesoporosity and acidity of the synthesized samples. The XRD results showed that MCM41 with high crystallinity. N2 adsorption indicated that BET surface area is 1300 m2•g－1. Pyridine TPD spectra of the samples showed that the acidity of MCM41 is a weak acid. The samples have high thermal stability. The optimum crystallization time is 50～100 h.
- MCM-41;Mesopore zeolite;Synthesis;Characterization
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