Citation:
Li Nan-Qiang, He Wei-Jun, Gu Zhen-Nan, Zhou Xi-Huang, Sun Yi-Liang, Wu Yong-Qing. Microelectrode Voltammetry for the Study of C60[J]. Acta Physico-Chimica Sinica,
;1994, 10(05): 399-401.
doi:
10.3866/PKU.WHXB19940505
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The microdisk electrode voltammetric behaviors of C_(60) are reported in this communication. This was accomplished by use of a mixed solvent system as Acetonotrile:Xylene=1:4 and a supporting electrolyte as 0.1 mol·L~(-1) Bu_4NPF_6. Au, Pt and Hg (Pt) were used as working electrode. In this new conditions, the successive six step reduction of C60 were obtained at below 15 ℃. It was found that the former five steps are all the single electron reversible reduction, but behaviors of the sixth steps are like EC' processes. Several electrochemical data were determined.
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Keywords:
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C60
, - Microdisk electrode,
- Voltammetry
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