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Citation: Liu Xiao-Lan, Sun Ming, Miao Fang-Ming, Li Yu-Gui, Wang Jian-Ji, Han Yu-Zhen, Xu Xiao-Jie. Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane[J]. Acta Physico-Chimica Sinica, ;1992, 8(01): 100-108. doi: 10.3866/PKU.WHXB19920118 shu

Crystal and Molecular Structure of 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane

1.
Chemistry Department, Tianjin Normal University, Tianjin 300074; Organo-Element Institute, Nankai University, Tianjin; Physical Chemistry Institute, Peking University, Beijing

Received Date: 11 May 1990
Available Online: 15 February 1992

The crystal structure of four 1-oxo-4-(substituent)-1-phospha-2,6,7-trioxacyclo(2,2,2) octane have been determinded by dimention single-crystal X-ray analysis.
All intensity data were collected with an Enraf-Nonius CAD4 diffractometer, using graphite monochromated Cu-K_α radiation and ω/2θ scan, and corrected for LP and emperical absorption factors. All crystal structures were solved by MULTAN and refined by full matrix least-squares with lsotropic thermal vibration factors for H and anisotropic for the others.
Crystal data, (I) X=NH, R=H, ...
- 1-Oxo-4-(Substituent)-1-Phospha-2,6,7-Trioxacyclo(2,2,2) Octane; Crystal structure
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