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Citation: Liu Xianyou, Zhou Lixing, Yin Anxue, Chen Shuxia, Zheng Lubin. THE CALORIMETRIC DEVICE FOR MEASUREMENT OF DIFFERENTIAL HEAT OF ADSORPTION IN GAS/SOLID SYSTEM[J]. Acta Physico-Chimica Sinica, ;1987, 3(03): 252-257. doi: 10.3866/PKU.WHXB19870307 shu

THE CALORIMETRIC DEVICE FOR MEASUREMENT OF DIFFERENTIAL HEAT OF ADSORPTION IN GAS/SOLID SYSTEM

1.
Dalia Institute of Chemical physics; Chinese Academy of Sciences

Received Date: 11 December 1985
Available Online: 15 June 1987

In this paper, high temperature calorimeter which is France SETARAM has been modified and introduced, Differential heats of adsorption for gas/solid system over the temperature range from ambient temperature to 800 K could be carried out in this apparatus, In the experimental procedure the amount of adsorption for gas or vapour could be measured by a light-spot microbarometer. The conversion factors for the apparatus have been determined through a electric-heating me- thod instead of standard materials which are usually used in temperature program process. By using this apparatus the heat of adsorption for pyrodine on H-Y zeolite at different temperatures have been measured.
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