Citation: HE Jincan, ZHANG Shiyun, SU Yuyuan, SONG Jiayi, WU Fuhai. Progress on the sample techniques and analytical methods for typical perfluorinated organic acids[J]. Chinese Journal of Chromatography, ;2020, 38(1): 86-94. doi: 10.3724/SP.J.1123.2019.06016 shu

Progress on the sample techniques and analytical methods for typical perfluorinated organic acids

School of Public Health, Guangdong Pharmaceutical University, Guangzhou 510310, China

Corresponding author: HE Jincan, hejincan300@163.com
Received Date: 19 June 2019

Fund Project: National Natural Science Foundation of China (No. 21804025)

Perfluorooctanesulfonate (PFOS) and perfluorooctanoic acid (PFOA) are typical perfluorinated organic acids with hepatotoxicity, embryonic toxicity, reproductive toxicity, and neurotoxicity. As the final degradation products of perfluorochemicals (PFCs) precursors, PFOS and PFOA are detected frequently. Presently, there are no unified standards for the detection of PFOS and PFOA. The analytical techniques used for PFCs in China are much less sophisticated than those in the developed countries. In this paper, the characteristics of PFOS and PFOA are introduced. Sample preparation technologies (liquid-liquid extraction, solid-phase extraction, solid-phase microextraction, ultrasonic extraction, and QuEChERS), and analytical methods (chromatography-mass spectrometry, spectrometry, ELISA, and electrochemical methods) are summarized and reviewed, so as to provide reference for monitoring and setting standards.
- perfluorochemicals (PFCs),
- perfluorooctanesulfonate (PFOS),
- perfluorooctanoic acid (PFOA),
- sample preparation,
- analytical methods,
- review
1. [1]
2. [2]
3. [3]
4. [4]
5. [5]
6. [6]
7. [7]
8. [8]
9. [9]
10. [10]
11. [11]
12. [12]
13. [13]
14. [14]
15. [15]
16. [16]
17. [17]
18. [18]
19. [19]
20. [20]
21. [21]
22. [22]
23. [23]
24. [24]
25. [25]
26. [26]
27. [27]
28. [28]
29. [29]
30. [30]
31. [31]
32. [32]
33. [33]
34. [34]
35. [35]
36. [36]
37. [37]
38. [38]
39. [39]
40. [40]
41. [41]
42. [42]
43. [43]
44. [44]
45. [45]
46. [46]
47. [47]
48. [48]
49. [49]
50. [50]
51. [51]
52. [52]
53. [53]
54. [54]
55. [55]
56. [56]
57. [57]
58. [58]
59. [59]
60. [60]
61. [61]
62. [62]
63. [63]
64. [64]
65. [65]
66. [66]
67. [67]
68. [68]
69. [69]
70. [70]
71. [71]
72. [72]
73. [73]
74. [74]
75. [75]
76. [76]
77. [77]
78. [78]
79. [79]
80. [80]
81. [81]
82. [82]
83. [83]
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