Citation: LIU Fan, GAO Fangyuan, TANG Tao, SUN Yuanshe, LI Tong, ZHANG Weibing. Analysis of amines in water samples by high performance liquid chromatography-laser induced fluorescence detection[J]. Chinese Journal of Chromatography, ;2013, 31(11): 1112-1115. doi: 10.3724/SP.J.1123.2013.09035 shu

Analysis of amines in water samples by high performance liquid chromatography-laser induced fluorescence detection

LIU Fan ¹ ,
GAO Fangyuan ¹ ,
TANG Tao ² ,
SUN Yuanshe ² ,
LI Tong ² ,
ZHANG Weibing ^1,,

1.
1. Shanghai Key Laboratory of Functional Materials Chemistry, East China University of Science and Technology, Shanghai 200237, China;

Corresponding author: ZHANG Weibing,
Received Date: 23 September 2013
Available Online: 29 September 2013
Fund Project: 国家重点基础研究发展规划("973")项目(2011CB910400,子课题2011CB910404) ("973")项目(2011CB910400,子课题2011CB910404)食品科学与技术国家重点实验室2010年度开放基金项目(SKLF-KF-201002) (SKLF-KF-201002)国家自然科学基金项目(21075039/B050106). (21075039/B050106)

A sensitive high performance liquid chromatography (HPLC)-laser induced fluorescence detection (LIFD) method was developed for the determination of amines. The derivatization and separation conditions were investigated. Under the optimized conditions, spermidine, putrescine and histamine were analyzed. The limits of detection (LODs) of the three biogenic amines (S/N=3) were as low as 10^-10 mol/L. This method showed excellent stability. The RSDs of retention times and peak areas of the three biogenic amines were lower than 0.3% and 3%, respectively. This method was applied in biogenic amine analysis in water samples, and the average recoveries were in the range of 94.99%-104.7%. Furthermore, the amines in seven tea samples were analyzed by this method, and satisfactory results were achieved. The developed assay is of excellent sensitivity and good reproducibility, which can be used in the analysis of the amines in water samples.
- high performance liquid chromatography (HPLC),
- laser induced fluorescence detection (LIFD),
- amines,
- water sample
1. [1]
  [1] Gan N, Li T H, Wang L Y, et al. Chinese Journal of Chromatography (干宁,李天华,王鲁雁,等. 色谱), 2007, 25(6): 934
2. [2]
  [2] Natividad G V, Javier S, Santiago H C. Anal Chim Acta, 2006, 575: 97
3. [3]
  [3] Qiao C D, Song P S, Yan X, et al. Chinese Journal of Analytical Chemistry(乔成栋,宋平顺,严祥,等. 分析化学),2007, 35(1): 95
4. [4]
  [4] Zhao X Y, Jiao X, Xia M, et al. Chinese Journal of Chromatography (赵新颖,焦霞,夏敏,刘清,等. 色谱), 2009, 27(4): 505
5. [5]
  [5] Zhang N, Wang H, Zhang Z X, et al. Talanta, 2008, 76: 791
6. [6]
  [6] Onal A. Food Chem, 2007, 103: 1475
7. [7]
  [7] Ding Z P, Liu C Q, Chen D, et al. Journal of Instrumental Analysis (丁卓平,刘辰麒,陈迪,等. 分析测试学报), 2006, 25(4): 59
8. [8]
  [8] Gosetti F, Mazzucco E, Gianotti V, et al. J Chromatogr A, 2007, 1149: 151
9. [9]
  [9] Liu X, Yang L X, Lu Y T. J Chromatogr A, 2003, 998: 213
10. [10]
  [10] Tseng H M, David A B. J Chromatogr A, 2009, 1216: 3387
11. [11]
  [11] Cao L W, Meng J X, Liu Y J. Chinese Journal of Analytical Chemistry (曹丽伟,孟健新,刘泳娟. 分析化学), 2008, 36(1): 24
12. [12]
  [12] Du M, Flanigan V, Ma Y F. Electrophoresis, 2004, 25:1496
13. [13]
  [13] Saito S T, Froehlich P E, Gosmann G, et al. Chromatographia, 2007, 65(9/10): 607
14. [14]
  [14] Huang X J, Huang Y, Wang J D, et al. Chinese Journal of Analytical Chemistry (黄晓佳, 黄颖, 王俊德, 等. 分析化学), 2005, 33(5): 627
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