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Citation: LIU Chunbo, ZENG Xiaoying, WANG Kunmiao, ZHAO Wei, HAN Jingmei, HE Pei, CHEN Yongkuan, MIAO Mingming, LIU Zhihua. Simultaneously Determining Thermal Decomposition Products of Pectin by a Combined Use of Simultaneous Thermal Analysis, FT-IR and GC-MS[J]. Chinese Journal of Applied Chemistry, ;2012, 29(10): 1218-1220. doi: 10.3724/SP.J.1095.2012.00572 shu

Simultaneously Determining Thermal Decomposition Products of Pectin by a Combined Use of Simultaneous Thermal Analysis, FT-IR and GC-MS

1.
a Key Laboratory of Tobacco Chemistry of Yunnan, Yunnan Academy of Tobacco Science, Kunming 650106, China;
2.
b Technology Centre of Hongyun Honghe Tobacco(Group) Co., Ltd, Kunming 650202, China

Corresponding author: LIU Zhihua,
Received Date: 27 December 2011
Available Online: 7 February 2012
Fund Project: 中国烟草总公司科技重大专项项目(110201001001) (110201001001)云南中烟工业公司科技开发计划(2010JC04) (2010JC04)云南省创新团队建设项目(2009CI014) (2009CI014)

A combination system of simultaneous thermal analysis(STA),Fourier-transform infrared(FT-IR) spectroscopy and GC-MS was established for simultaneously determination of pyrolysised products of the pectin samples under nitrogen or nitrogen-oxygen atmosphere.According to the pyrolysis behavior of pectin,26 substances were detected at three temperatures(243℃,270℃ and 335℃) on line with the system.
- simultaneous thermal analysis,
- FT-IR,
- GC-MS,
- pectin pyrolysis
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