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Citation: LI Yuan, LI Guijuan, DING Mengxian, WANG Zhen. Preparation and Performance of Bisphenol F-Type Polyimide Films[J]. Chinese Journal of Applied Chemistry, ;2011, 28(12): 1370-1374. doi: 10.3724/SP.J.1095.2011.00754 shu

Preparation and Performance of Bisphenol F-Type Polyimide Films

LI Yuan ^a ,
LI Guijuan ^a ,
DING Mengxian ^b,c ,
WANG Zhen ^c,,

1.
a School of Chemical Engineering, Changchun University of Technology, Changchun;
2.
b The Company of Gaoqi Polyimides Material, Changchun;
3.
cChangchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022

Corresponding author: WANG Zhen,
Received Date: 23 December 2010
Available Online: 11 April 2011
Fund Project: 国家重点基础研究发展计划(2010CB631100) (2010CB631100)吉林省科技发展计划项目(20080110)资助 (20080110)

A novel bisphenol F-type dianhydride(BPFDA) monomer was synthesized using 4-chlorophthalimide through hydration,acidification,and dehydration.Its structure was determined with ¹H NMR and IR.Two types of polyimide films were prepared with the dianhydride and 4,4'-diaminodiphenyl ether(ODA) or 4,4'-methylene dianiline(MDA) via conventional one-step method in N,N'-dimethylacetamide.The obtained polyamic acid was then further imidized into polyimide films and characterized.Results show that the glasstransition temperatures of the polyimide films were 200 and 204℃;the temperatures of 5% mass loss were 506.50 and 459.10℃;and the tensile strength of the films were 110 and 100 MPa,respectively.
- bisphenol F-type dianhydride,
- polyimide,
- thermal property,
- mechanical properties
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