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Citation: ZHANG Kai, BAI Hongmei, CHENG Fangyi, CHEN Jun. Preparation of Sn Films by Vacuum Evaporation and Their Electrochemical Properties as Lithium-Storage Materials[J]. Chinese Journal of Applied Chemistry, ;2011, 28(8): 918-923. doi: 10.3724/SP.J.1095.2011.00595 shu

Preparation of Sn Films by Vacuum Evaporation and Their Electrochemical Properties as Lithium-Storage Materials

1.
Institute of New Energy and Material Chemistry, Key Laboratory of Advanced Energy Materials Chemistry-Ministry of Education, Nankai University, Tianjin 300071

Corresponding author: CHEN Jun,
Received Date: 10 October 2010
Available Online: 18 November 2010
Fund Project: 国家自然科学基金(20873071) (20873071)天津应用基础及前沿技术研究(08JCZDJC21300)资助项目 (08JCZDJC21300)

Sn thin films on Cu foil substrate were prepared by vacuum evaporation and investigated as the anode materials of rechargeable lithium-ion batteries.The surface morphology and composition of the asprepared films were characterized by scanning electron microscopy(SEM) and X-ray diffraction(XRD).The electrochemical performance of the film electrodes was measured using CR2032 coin-type cells.The experimental results show that the deposited films are composed of nano/micro particles,which are enlarged with increasing both the evaporation power and the substrate temperature.This behavior is correlated with the electrochemical performance of the film electrode.It is found that at 200 W and 150℃,the thin film with small particle of Cu₆Sn₅ phase displays a discharge capacity of 527 mA·h/g after 20 cycles.
- tin film,
- vacuum evaporation,
- lithium-ion battery,
- anode material
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