Citation: LI Hui-Min, ZHOU Yu-Chen, XIAO Yu-Fang, FAN Jing, FENG Su-Ling, XU Sheng-Rui. Application of Cooling-assisted Solid Phase Microextraction in Analysis of Complex Matrix Sample[J]. Chinese Journal of Analytical Chemistry, ;2022, 50(9): 1289-1298. doi: 10.19756/j.issn.0253-3820.221157 shu

Application of Cooling-assisted Solid Phase Microextraction in Analysis of Complex Matrix Sample

LI Hui-Min ¹ ,
ZHOU Yu-Chen ² ,
XIAO Yu-Fang ² ,
FAN Jing ^3,, ,
FENG Su-Ling ¹ ,
XU Sheng-Rui ^1,3,,

1.
School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang 453007, China;
2.
Hubei Province Geological Experimental Testing Center, Wuhan 430034, China;
3.
School of Environment, Henan Normal University, Xinxiang 453007, China

Corresponding author: FAN Jing, XU Sheng-Rui,
Received Date: 31 March 2022
Revised Date: 1 June 2022

Fund Project: Supported by the National Natural Science Foundation of China (Nos.21976052, 21705017) and the Youth Science Foundation of Henan Normal University (No.20200183).

The green sample pretreatment technique has been one of the research hotspots in the analysis of complex matrix samples. Although solvent-free extraction of volatile organic compounds in samples can be implemented by headspace solid-phase microextraction (HS-SPME), it is difficult to achieve satisfactory results for complex matrix samples. Cooling-assisted solid phase microextraction (CA-SPME) allows for heating sample matrix and cooling coating simultaneously, which overcomes the drawbacks of regular HS-SPME, and effectively promotes the extraction efficiency for volatile and semi-volatile compounds in complex matrix samples. Thus, the solvent-free sample analysis in complex matrix can be accomplished by CA-SPME. Given its unique advantages, CA-SPME provides a new approach for green sample analysis from complex matrix. Therefore, the recent advances of CA-SPME were introduced in this review, including the studies in CA-SPME devices, the factors affecting extraction efficiency, and the applications of CA-SPME. Finally, the future trends and prospective were also discussed. This review aimed to provide a valuable reference for research in complex sample analysis.
- Cooling-assisted solid phase microextraction,
- Sample preparation,
- Complex matrix,
- Review
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