Citation: LONG Mei-Ming, HU Yu-Fei, LI Gong-Ke. Cataluminescence Method for Rapid Identification of Refreshing Powder[J]. Chinese Journal of Analytical Chemistry, ;2022, 50(7): 1057-1064. doi: 10.19756/j.issn.0253-3820.221000 shu

Cataluminescence Method for Rapid Identification of Refreshing Powder

School of Chemistry, Sun Yat-sen University, Guangzhou 510006, China

Corresponding author: HU Yu-Fei, LI Gong-Ke,
Received Date: 2 January 2022
Revised Date: 17 April 2022

Fund Project: Supported by the National Natural Science Foundation of China (Nos.21775167, 21976213) and the State Key Program of the National Natural Science Foundation of China(No.22134007).

Volatile organic compounds can produce chemiluminescence on the surface of talc powder and refreshing powder. Under the optimal conditions, including reaction temperature of 210℃, detection wavelength of 425 nm and flow rate of carrier gas at 300 mL/min, there was a good linear relationship between the CTL signal intensity on talc surface and the concentration of n-propanal, and the slope (k) of linear regression equation could be used as the characteristic value for identification of talc powder. If n-propanal could not produce obvious CTL signal on the surface of some talc powder or could produce CTL signal but the k value was relatively close, then the CTL signals of six volatile organic compounds on the surface of talc powder were normalized and coded in sequence, and each talc powder corresponded to a digital coding, which could be used for identification of refreshing powder. The two methods abovementioned were successfully used for identification of 12 brands of refreshing powders. The k values of seven batches of the same refreshing powder were investigated, with RSD of 3.1%, showing excellent stability. Moreover, the method was verified to be fast and accurate by linear discriminant analysis.
- Talc powder,
- Refreshing powder,
- Volatile organic compounds,
- Cataluminescence,
- Identification
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