Citation: ZHANG Xin, LI Yan-Song, HAN Rui, JIANG Yan-Yan, LIU Zhe-Han. Construction of Molecularly Imprinted Photonic Crystal Sensor for Detection of Bisphenol A and Dicyandiamide[J]. Chinese Journal of Analytical Chemistry, ;2020, 48(3): 389-395. doi: 10.19756/j.issn.0253-3820.191684 shu

Construction of Molecularly Imprinted Photonic Crystal Sensor for Detection of Bisphenol A and Dicyandiamide

1.
School of Life Science and Technology, Nanyang Normal University, Nanyang 473061, China;
2.
School of Life Science, Beijing Institute of Technology, Beijing 100081, China

Received Date: 19 November 2019
Revised Date: 2 January 2020

Fund Project: This work was supported by the Key Scientific Research Projects of Higher Education Institutions in Henan Province, China (No. 20A180021) and the Scientific Research Projects of Nanyang Normal University (No. 2019ZX011).

The molecular imprinting technique and photonic crystal materials were combined to construct an array of sensors based on inverse-opal structure molecularly imprinted photonic crystal film (MIPPs) for the determination of trace amounts of bisphenol A (BPA) and dicandiamide (DCD) in environmental water samples. The polymerization system of molecularly imprinting and elution system were optimized. The best adsorptive property and the maximum diffraction peak of the prepared BPA and DCD molecularly imprinted photonic crystal film were achieved when the ratios of monomer and template molecules were 1:2 and 1:4, respectively. The performance of the MIPPs sensor array was investigated by adsorption kinetics and adsorption isotherm experiments. Experimental results showed that the response time of the prepared MIPPs for BPA and DCD were 2.5 and 4.0 min, respectively. In the concentration range of 0.1-5.0 μg/L and 0.1-10.0 μg/L, the diffraction peak displacement of MIPPs for BPA and DCD was obvious, the maximum displacement was 39 and 31 nm, and the limits of detection were 0.051 μg/L and 0.038 μg/L(S/N=3), respectively. However, the diffraction peak displacement of the non-imprinted photonic crystal film was not obvious, which indicated that the prepared MIPPs had selective specificity. The real sample test results showed that the development MIPPs had an obvious optical signal response to the target molecules, which could be used for the rapid, sensitive and selective detection of the residual BPA and DCD in environmental waters.
- Molecular imprinting,
- Photonic crystal,
- Sensor array,
- Bisphenol A,
- Dicandiamide
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沈阳化工大学材料科学与工程学院沈阳 110142