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Citation: Xiao-Wei MA, Hai-Feng LIN, Yan-Yan LI, Lei WANG, Xi-Peng PU, Xiu-Jie YI. Dramatically Enhanced Visible-light-responsive H2 Evolution of Cd1-xZnxS via the Synergistic Effect of Ni2P and 1T/2H MoS2 Cocatalysts[J]. Chinese Journal of Structural Chemistry, ;2021, 40(1): 7-22. doi: 10.14102/j.cnki.0254-5861.2011-2752 shu

Dramatically Enhanced Visible-light-responsive H2 Evolution of Cd1-xZnxS via the Synergistic Effect of Ni2P and 1T/2H MoS2 Cocatalysts

  • a.

    College of Materials Science and Engineering, Liaocheng University, Liaocheng 252059, China

  • b.

    Key Laboratory of Eco-chemical Engineering, Taishan Scholar Advantage and Characteristic Discipline Team of Eco-chemical Process and Technology, College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042, China

  • Corresponding author: Yan-Yan LI, liyanyan6771@163.com Xi-Peng PU, xipengpu@lctu.edu.cn Xiu-Jie YI, yixiujie@126.com
  • Received Date: 2 February 2020
    Accepted Date: 27 February 2020

    Fund Project: the Foundation of State Key Laboratory of Structural Chemistry 20190021the National Natural Science Foundation of China 51802170the National Natural Science Foundation of China 21801150the National Natural Science Foundation of China 51772162the Natural Science Foundation of Shandong Province ZR2018BEM014the Natural Science Foundation of Shandong Province ZR2019JQ14the Natural Science Foundation of Shandong Province ZR2019MB001

Figures(13)

  • Photocatalytic hydrogen generation from water-splitting holds huge promise for resolving the current energy shortage and environmental issues. Nevertheless, it is still challenging so far to develop non-noble-metal photocatalysts which are efficient toward solar-powered hydrogen evolution reaction (HER). In this work, through an ultrasonic water-bath strategy combined with solvothermal and electrostatic assembly processes, we obtain homogeneous Cd1-xZnxS–Ni2P–MoS2 hybrid nano-spheres consisting of Cd1-xZnxS solid solutions decorated by Ni2P and 1T/2H MoS2 cocatalysts, which demonstrate excellent activity and stability for visible-light-responsive (λ > 420 nm) H2 production. Specifically, the Cd1-xZnxS–Ni2P–MoS2 nano-spheres with 2 wt% Ni2P and 0.2 wt% MoS2 (CZ0.7S–2N–0.2M) exhibit the optimal HER activity of 55.77 mmol∙g-1∙h-1, about 47 and 32 times more than that of CZ0.7S and Pt–CZ0.7S, respectively. The outstanding HER performance of Cd1-xZnxS–Ni2P–MoS2 can be ascribed to the presence of abundant HER active sites in Ni2P nanoparticles and 1T/2H MoS2 nanosheets as well as the effective transfer and separation of charge carriers. Moreover, the coupling sequence of cocatalysts in Cd1-xZnxS–Ni2P–MoS2 is found to be critical in the regulation of charge transfer pathways and thus the resultant photocatalytic efficiency. The results displayed here could facilitate the engineering of high-performance photocatalysts employing multi-component cocatalysts for sustainable solar-to-fuel conversion.
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