Citation: WANG Jian-Fang, WU Ya-Pan, WU Xue-Qian, WEN Guo-Xuan, WANG Chao. One New 3D Pillared-layer Ag(I)-Coordination Framework Based on a Unique 1D Ag₂O₂ Ribbon: Synthesis, Crystal Structure and Luminescent Properties[J]. Chinese Journal of Structural Chemistry, ;2016, 35(8): 1238-1244. doi: 10.14102/j.cnki.0254-5861.2011-1040 shu

One New 3D Pillared-layer Ag(I)-Coordination Framework Based on a Unique 1D Ag₂O₂ Ribbon: Synthesis, Crystal Structure and Luminescent Properties

1.
a College of Materials and Chemical Engineering, Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials, China Three Gorges University, Yichang 443002, China;
2.
b Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of the Ministry of Education, College of Chemistry & Materials Science, Northwest University, Xi'an 710069, China

Corresponding author: WU Ya-Pan,
Received Date: 3 November 2015
Available Online: 21 March 2016
Fund Project: This project was supported by the NSF of Hubei Province (No. 2014CFB277) (No. 2014CFB277)

A new 3D Ag(I) coordination polymer {[Ag(AZDB)_0.5(bpe)_0.5]·H₂O}_n (1) has been papared by azobenzene-3,3'-dicarboxylicate (H₂AZDB), 1,2-bis(4-pyridyl)ethylene (bpe) and silver salts via hydrothermal method. The compound was fully characterized by single-crystal X-ray diffraction, elemental analyses, infrared spectrum (IR), powder X-ray diffraction (PXRD) and thermogravimetric analysis (TGA). The strucrural analysis indicate that compound 1 shows a 3D pillared-layer framework constructed from a unique 1D Ag₂O₂ ribbon and pyridyl/carboxylicate mixed system, which features a 2-nodal (4, 6)-connected fsc net with a (4⁴·6¹⁰·8)(4⁴·6²) topology. Moreover, the photoluminescent properties have also been discussed.
- Ag(I) coordination polymer,
- 3D pillared-layer framework,
- 1D Ag₂O₂ ribbon,
- fsc topology
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