Citation: DONG Yilin, ZHANG Hao, CHEN Jinlong. Preparation of Cosmetic-Grade Sodium Polyaspartate[J]. Chinese Journal of Applied Chemistry, ;2020, 37(8): 883-888. doi: 10.11944/j.issn.1000-0518.2020.08.200062 shu

Preparation of Cosmetic-Grade Sodium Polyaspartate

DONG Yilin ^a,b ,
ZHANG Hao ^a ,
CHEN Jinlong ^b,,

a.
College of Food Science and Engineering, Jilin Agricultural University, Changchun 130118, China
b.
Key Laboratory of Polymer Ecomaterials, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China

Corresponding author: CHEN Jinlong, chenjl2015@ciac.ac.cn
Received Date: 10 March 2020
Revised Date: 15 April 2020
Accepted Date: 9 May 2020

Fund Project: Supported by the National Natural Science Foundation of China(No.21805272, No.31801477)the National Natural Science Foundation of China 21805272the National Natural Science Foundation of China 31801477

Figures(7)

Cosmetic-grade sodium polyaspartate was synthesized through the polycondensation of L-aspartic acid. The effects of polymerization temperature, time and catalyst amount on the polymerization were systematically investigated to obtain the optimal polymerization conditions. The structure and molecular weight of sodium polyaspartate were characterized by nuclear magnetic resonance spectroscopy (NMR) and gel permeation chromatography (GPC). The properties of acid and alkali resistance, temperature resistance and compatibility were also evaluated. The resultant sodium polyaspartate has light color (white), low odor, few impurities and high quality, exhibits excellent acid, alkali, temperature resistance and compatibility, reaches the standard as a moisturizing additive.
- L-aspartic acid,
- sodium polyaspartate,
- condensation polymerization
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