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Citation: JIAO Liansheng, MENG Lingju, WU Tongshun, LI Fenghua, NIU Li. Synthesis and Properties of Lithium Vanadium Phosphates/Reduced Graphene Oxide Composite as Cathode Materials[J]. Chinese Journal of Applied Chemistry, ;2017, 34(6): 712-722. doi: 10.11944/j.issn.1000-0518.2017.06.160357 shu

Synthesis and Properties of Lithium Vanadium Phosphates/Reduced Graphene Oxide Composite as Cathode Materials

  • a.

    State Key Laboratory of Electroanalytical Chemistry, c/o Engineering Laboratory for Modern Analytical Techniques, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China

  • b.

    University of Chinese Academy of Sciences, Beijing 100049, China

  • c.

    Department of Chemistry, Hebei Normal University for Nationalities, Chengde, Hebei 067000, China

  • d.

    School of Chemistry & Chemical Engineering, Linyi University, Linyi, Shandong 276005, China

  • Corresponding author: NIU Li, lniu@ciac.ac.cn
  • Received Date: 6 September 2016
    Revised Date: 10 October 2016
    Accepted Date: 2 December 2016

    Fund Project: Fund for Major Research Instruments and Equipment Development NSFC 215278106the Taishan Scholar Project ts201511058the National Science Fund for Distinguished Young Scholars NSFC 21225524

Figures(10)

  • Lithium vanadium phosphate(Li3V2(PO4)3)/reduced graphene oxide(rGO) composite has been successfully synthesized by incorporating melamine resin(MR) functionalized GO precursor into the Li3V2(PO4)3 solution and the subsequent heat treatment. The structural and electrochemical properties of Li3V2(PO4)3/rGO were characterized. The results show that Li3V2(PO4)3/rGO composite has monoclinic system, restacking of graphene layers and agglomeration of Li3V2(PO4)3 particles have been greatly inhibited, electrochemical performance of the composite has been improved. The as-obtained Li3V2(PO4)3/rGO was used as the cathode material in lithium ion batteries. The very low degree of polarization in the curve shows that electron and ion transports are facile, thus good rate and cycle behavior are observed. A considerably high lithiation capacity of 86 mA·h/g can be retained even at 20 C in the range of 3.0~4.3 V. After 100 cycles at 0.1 C, a discharge capacity of 119.7 mA·h/g could be delivered with the capacity retention of 94%. When the cells are operated between the voltage limits of 3.0~4.8 V vs.Li+/Li, a lithiation capacity of 80 mA·h/g at 10 C and 145.6 mA·h/g at 0.1 C after 100 cycles could be retained. Good cycling and rate performances, together with low carbon content, will be satisfactory for use as cathode material in lithium ion batteries.
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