Citation: WU Liqiong, HAO Lihua, KONG Fanhua, LI Xinheng. Confined In-Situ Synthesis of Ferroferric Oxide Nanoparticles on Mesoporous Carbon[J]. Chinese Journal of Applied Chemistry, ;2016, 33(11): 1340-1342. doi: 10.11944/j.issn.1000-0518.2016.11.160148 shu

Confined In-Situ Synthesis of Ferroferric Oxide Nanoparticles on Mesoporous Carbon

1.
State Key Laboratory for Oxo Synthesis and Selective Oxidation, Suzhou Research Institute of LICP, Lanzhou Institute of Chemical Physics(LICP), Chinese Academy of Sciences, Suzhou, Jiangsu 215123, China

Corresponding author: KONG Fanhua, LI Xinheng,
Received Date: 11 April 2016
Available Online: 8 June 2016
Fund Project:

Mesoporous carbon with monolithic structures were prepared using abandoned crab shells as a template. And then Fe₃O₄ nanoparticles inside those monolithic mesopores were synthesized by the confined in-situ synthetic strategy. The properties and structure of Fe₃O₄ nanoparticles on nesoporous narbon were characterized by scanning electronic microscopy(SEM), transmission electron microscope(TEM) and X-ray diffraction(XRD). The results show that the pores have a monolithic structure. The diameters of the pores are ca. 40~50 nm and their lengths are ca. 50 μm to 200 μm. The nanoparticles are proven to be Fe₃O₄ with 10 nm in diameter, which have good size monodispersity and are evenly distributed inside the pores. This method features simple and environmental benignity.
- Fischer-Tropsch synthesis,
- nanocatalysis,
- iron oxide,
- porous carbon,
- monolithic structures
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沈阳化工大学材料科学与工程学院沈阳 110142