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Citation: SUN Linlin, ZHOU Yehong, WANG Fei, SHUANG Shaomin, DONG Chuan. Adsorption Properties of Carboxymethyl-β-cyclodextrin Functionalized Ferroferric Oxide Magnetic Nanocomposites on Rhodamine B[J]. Chinese Journal of Applied Chemistry, ;2015, 32(1): 110-117. doi: 10.11944/j.issn.1000-0518.2015.01.140147 shu

Adsorption Properties of Carboxymethyl-β-cyclodextrin Functionalized Ferroferric Oxide Magnetic Nanocomposites on Rhodamine B

1.
Institute of Environmental Science, College of Environmental and Resource Sciences, Shanxi University, Taiyuan 030006, China

Corresponding author: DONG Chuan,
Received Date: 25 April 2014
Available Online: 24 June 2014
Fund Project: 国家自然科学基金(21175086)资助项目 (21175086)

Carboxymethyl-β-cyclodextrin (CM-β-CD) synthesized by S_N 2 substitution was employed successfully on the modification of the surface of the Fe₃O₄ magnetic nanoparticles(MNPs) using a layer-bylayer method. The as-prepared CM-β-CD functionalized magnetic nanocomposites (CM-β-CD-MNPs) were characterized by transmission electron microscopy(TEM),Fourier transform infrared spectroscopy(FTIR) and vibrating sample magnetometer(VAM). The adsorption properties of CM-β-CD-MNPs on rhodamine B(RhB) were investigated. The results show that CM-β-CD-MNPs are nearly spherical,with an average particle diameter of 16 nm,and are superparamagnetic with a relatively high saturation magnetization value of 54 emu/g. Adsorption kinetic coincides with the pseudo-second-order kinetic model and the adsorption equilibrium is reached within 1 h. Adsorption isotherm fits well to Langmuir adsorption model and the maximum adsorption reaches up to 135.1 mg/g.
- carboxymethyl-β-cyclodextrin,
- ferroferric oxide,
- adsorption,
- rhodamine B
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