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Citation: LUO Rui-Ping, ZHENG Ling-Na, LI Liang, WANG Juan, FENG Wei-Yue, YU Xiang-Hua, WANG Meng. Effect of Data Acquisition Parameters on Characterization of Gold Nanoparticles By Single Particle Inductively Coupled Plasma-Mass Spectrometry[J]. Chinese Journal of Analytical Chemistry, ;2018, 46(6): 925-930. doi: 10.11895/j.issn.0253-3820.181059 shu

Effect of Data Acquisition Parameters on Characterization of Gold Nanoparticles By Single Particle Inductively Coupled Plasma-Mass Spectrometry

LUO Rui-Ping ^1,2, ,
ZHENG Ling-Na ^2,3 ,
LI Liang ¹ ,
WANG Juan ⁴ ,
FENG Wei-Yue ² ,
YU Xiang-Hua ¹ ,
WANG Meng ²

1.
School of Material Science and Engineering, Wuhan Institute of Technology, Wuhan 430205, China;
2.
Key Laboratory for Biomedical Effects of Nanomaterials and Nanosafety, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049, China;
3.
University of Chinese Academy of Sciences, Beijing 100049, China;
4.
Perkin Elmer Management Shanghai Co., Ltd., Shanghai 201203, China

Received Date: 25 January 2018
Revised Date: 22 March 2018

Fund Project: This work was supported by the National Natural Science Foundation of China (Nos. 11505194, U1432241) and the National Basic Research Program of China (No. 2016YFA0201604).

Single particle inductively coupled plasma mass spectrometry (SP-ICP-MS) is a new tool that can provide the element composition, size distribution, and number concentration of nanoparticles. Here we discussed the effects of dwell time and settling time on analysis of nanoparticles by SP-ICP-MS. We analyzed standard materials of gold nanoparticles (30, 40 and 60 nm AuNPs, from NIST and NCNST), showing that better signal-to-noise ratio and higher determination efficiency could be achived when using shorter dwell time and settling time. We utilized a nano mode for SP-ICP-MS, in which the dwell time was set as 0.05 ms and the settling time was 0. The size of NIST AuNP standard material determined here was in accord with the certified size using the developed method. The detection limits of size and number concentration of AuNPs were 8 nm and 1.1×10⁵ particle/L, respectively.
- Gold nanoparticles,
- Single particle inductively coupled plasma mass spectrometry,
- Dwell time,
- Settling time
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