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Citation: ZHANG Pei-Xu, JIN Yong-Ri, CUI Li, WU Qian, LI Peng, ZHANG Han-Qi, LI Xu-Wen. Extraction of Eight Ginsenosides from Leaves of Panax quinquefolium L. By Ultrasoinc Fountain-based Ultrasonic-assisted Nebulization Extraction Coupled with Solid Phase Extraction[J]. Chinese Journal of Analytical Chemistry, ;2018, 46(4): 594-600. doi: 10.11895/j.issn.0253-3820.171117 shu

Extraction of Eight Ginsenosides from Leaves of Panax quinquefolium L. By Ultrasoinc Fountain-based Ultrasonic-assisted Nebulization Extraction Coupled with Solid Phase Extraction

ZHANG Pei-Xu ^1,2, ,
JIN Yong-Ri ¹ ,
CUI Li ² ,
WU Qian ¹ ,
LI Peng ¹ ,
ZHANG Han-Qi ¹ ,
LI Xu-Wen ¹

1.
College of Chemistry, Jilin University, Changchun 130021, China;
2.
Department of Neurology, First Hospital, Jilin University, Changchun, 130021, China

Received Date: 21 July 2017
Revised Date: 21 January 2018

A new ultrasonic-assisted extraction (UANE) method coupled with solid phase extraction (SPE) using ultrasonic fountain was established for the extraction of eight common ginsenosides from leaves of Panax quinquefolium L. The extraction system has been designed and several experimental parameters, including the type and volume of extraction solvent, pH value and salt concentration of extraction solvent,type and volume of elution solvent,and amount of C₁₈, extraction time were examined and optimized. Under the optimal conditions, the recoveries of ginsenosides were in the range of 96.3%-110.6%, the relative standard deviations (RSDs) were in the range of 2.8%-4.3%, indicating that the method has a good performance for the extraction of these ginsenosides. Compared with traditional UANE-SPE method, the modified method simplified the extraction device, shortened the extraction time and improved the extraction efficiency.
- Ultrasonic-assisted nebulization extraction,
- Solid phase extraction,
- Ultrasonic fountain,
- Panax quinquefolium L.,
- Ginsenosides
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