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Citation: ZHANG Zhong-Xiang, ZHAO Qi, LIU Yu-Lei, MA Jun, QI Jing-Yao, REN Zhi-Jun. Determination of Twelve Kinds of Volatile Disinfection Byproducts in Drinking Water by Gas Chromatography with Electron Capture Detector[J]. Chinese Journal of Analytical Chemistry, ;2017, 45(8): 1203-1208. doi: 10.11895/j.issn.0253-3820.170142 shu

Determination of Twelve Kinds of Volatile Disinfection Byproducts in Drinking Water by Gas Chromatography with Electron Capture Detector

1.
School of Municipal and Environmental Engineering, Harbin Institute of Technology, Harbin 150001, China;2 School of Energy and Environmental Engineering, Hebei University of Technology, Tianjin 300401, China

Received Date: 10 March 2017
Revised Date: 12 June 2017

Fund Project: This work was supported by the National Natural Science Foundation of China (No.51378141),and the Program of State Key Laboratory of Urban Water Resource and Environment (HIT)(No.2016DX04).

A method for simultaneous determination of 12 kinds of chlorinated disinfection byproducts (DBPs) in drinking water was developed based on liquid-liquid extraction gas chromatography equipped with electron capture detector (GC/ECD). The procedural standard calibration was adopted to eliminate the interference of different matrix. The method detection limits for 12 DBPs were 0.08-0.21 μg/L and the entire analytical procedure was finished in 21.50 min. The recoveries were in the range of 80.9%-115.7% and the relative standard deviations (RSD) were between 0.9% and 9.9% at different concentration levels (5 and 50 μg/L) in tap water and surface water. The correlation coefficients for all 12 kinds of DBPs were greater than 0.99 in the linearity range of 0.5-200 μg/L. The method was applied to determine DBPs in drinking water and source water. This method was rapid and competent for detection of volatile DBPs in drinking water.
- Disinfection byproducts,
- Gas Chromatography,
- Volatile,
- Chlorine disinfection,
- Drinking water
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