Citation: ZHAO Wen-Bin, WANG Meng-Fan, ZENG Chuan, QI Wei, SU Rong-Xin, HE Zhi-Min. Surface Enhanced Raman Scattering Substrate Base on Band Gap Edge Effect of Photonic Crystal[J]. Chinese Journal of Analytical Chemistry, ;2017, 45(6): 906-913. doi: 10.11895/j.issn.0253-3820.170023 shu

Surface Enhanced Raman Scattering Substrate Base on Band Gap Edge Effect of Photonic Crystal

ZHAO Wen-Bin ^1, ,
WANG Meng-Fan ^1,3 ,
ZENG Chuan ⁴ ,
QI Wei ^1,2,3 ,
SU Rong-Xin ^1,2,3 ,
HE Zhi-Min ¹

1.
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China;
2.
State Key Laboratory of Chemical Engineering, Tianjin University, Tianjin 300072, China;
3.
Tianjin Key Laboratory of Membrane Science and Desalination Technology, Tianjin 300072, China;
4.
Technical Center of Zhuhai Inspection & Quarantine Bureau, Zhuhai 519000, Guangdong, China

Received Date: 12 January 2017
Revised Date: 6 April 2017

Fund Project: This work was supported by the National Natural Science Foundation of China (Nos.21676191,21621004) and the National Major Scientific Instruments and Equipments Special Project (No.2012YQ090194)

In this work, band gap edge effect of photonic crystal (PC) was combined with gold nanoparticles (AuNPs) to fabricate a novel surface enhanced Raman scattering (SERS) substrate (PC-AuNPs). The preparation of PC-AuNPs substrate consisted of three steps. Firstly, SiO₂ nanospheres were amino-modified. Then, an opal PC structure was obtained by vertical deposition of SiO₂ nanospheres. Finally, AuNPs were loaded on the surface of opal structure. The Raman scattering signal of Rhodamine B (RhB) was detected on PC-AuNPs to evaluate the merits of this new substrate. It was found that the band gap range of photonic crystal and the loading amount of AuNPs were important factors for PC-AuNPs. A good linearity relationship could be obtained between the characteristic peak intensity of RhB and its logarithmic concentration (I=1711lg[RhB (mol/L)]+15244, R²=0.9994). The detection limit reached 1×10^-8 mol/L. This method was simple and exhibited good sensitivity and reproducibility for Raman scattering detection, and could provide a novel strategy for the development of SERS substrate.
- Surface enhanced Raman scattering,
- Photonic crystal,
- Band edge effect,
- Gold nanoparticles
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