Citation: HU Peng, NIU Jing, YU Miao, LIN Shuang-Yan. Facile Solvothermal Synthesis of Reduced Graphene Oxide-BiPO₄ Nanocomposite with Enhanced Photocatalytic Activity[J]. Chinese Journal of Analytical Chemistry, ;2017, 45(3): 357-362. doi: 10.11895/j.issn.0253-3820.160734 shu

Facile Solvothermal Synthesis of Reduced Graphene Oxide-BiPO₄ Nanocomposite with Enhanced Photocatalytic Activity

HU Peng ^1, ,
NIU Jing ¹ ,
YU Miao ¹ ,
LIN Shuang-Yan ²

1.
College of Chemistry and Pharmaceutical Engineering, HuangHuai University, Zhumadian 463000, China;
2.
Physics and Electronic Engineering College, Harbin Normal University, Harbin 150025, China

Received Date: 29 September 2016
Revised Date: 23 December 2016

Fund Project: This work was supported by the Scientific and Technological Project of Henan Province (No. 162102310262), the Key Project of Colleges in Henan (No. 16A150015) and the Open Project Program of Key Laboratory for Photonic and Electric Bandgap Materials, Ministry of Education, Harbin Normal University, China (No. PEBM201510)

Reduced graphene oxide-BiPO₄ (RGO-BiPO₄) nanocomposite was synthesized successfully via a one-pot solvothermal method using graphene oxide and bismuth nitrate as precursors and glycerin as solvent at 200℃ for 1 h. The morphology and structure of as-prepared nanocomposite were characterized by SEM, TEM, XRD, XPS, SERS and UV-Visible spectrum. The photocatalytic activity of the nanocomposite was evaluated by the photodegradation of Rhodamine B (RhB) dye under UV irradiation and it was found that RGO-BiPO₄ nanocomposite possessed higher photocatalytic activity than that of pure BiPO₄. RhB could be decomposed 87.5% within 2 h. Under the same conditions, only 45.7% of the RhB dye could be decomposed by BiPO₄. The enhancement of photocatalytic activity could be attributed to the effective charge separation due to the electron-accepting and transporting properties of graphene.
- Reduced graphene oxide,
- BiPO₄,
- Nanocomposite,
- Photocatalytic activity,
- Rhodamine B
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Facile Solvothermal Synthesis of Reduced Graphene Oxide-BiPO4 Nanocomposite with Enhanced Photocatalytic Activity

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通讯作者: 陈斌, bchen63@163.com

Facile Solvothermal Synthesis of Reduced Graphene Oxide-BiPO₄ Nanocomposite with Enhanced Photocatalytic Activity