Citation: LONG Tao, SHI Jian, BAO Ze-Min, Stephen W. J. Clement, ZHANG Yu-Hai, TIAN Di, LIU Dun-Yi. Influence of Edge Effect and X-Y Effect on Measurement Precision in Sensitive High Resolution Ion Microprobe IIe MC Oxygen Isotopes Analysis[J]. Chinese Journal of Analytical Chemistry, ;2015, 43(12): 1888-1894. doi: 10.11895/j.issn.0253-3820.150581 shu

Influence of Edge Effect and X-Y Effect on Measurement Precision in Sensitive High Resolution Ion Microprobe IIe MC Oxygen Isotopes Analysis

1.
¹ Department of Instrumentation & Electrical Engineering, Jilin University, Changchun 130026, China;

Corresponding author: LONG Tao,
Received Date: 21 July 2015
Available Online: 11 September 2015
Fund Project: 本文系国家重大科学仪器设备开发专项资助(No.2011YQ05006902) (No.2011YQ05006902)

Sensitive high resolution ion microprobe(SHRIMP) IIe MC has been widely used in the oxygen isotopes analysis of zircon, apatite, calcium carbonate, etc.. This study provides guidance for SHRIMP IIe MC high precision O-isotope analysis. We have established the secondary ion extraction structure of SIMION simulation model and discussed the cause and influencing factors of edge effect and X-Y effect in oxygen isotopes analysis. Higher δ¹⁸O precision can be reached by limiting O-isotope analysis position(the sample is located at the center of the mount within 10 mm diameter and the target surface roughness is less than 1μm). The internal precision of single spot of zircon δ¹⁸O is better than 0.15‰(1σ), with external precision better than 0.5%(95% confidence); the internal precision of the single analysis of Carbonate δ¹⁸O is better than 0.20‰(1σ), with external precision better than 0.6‰(95% confidence).
- Sensitive high resolution ion microprobe,
- Oxygen analysis,
- Edge effect,
- X-Y effect
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