Citation: Mochou GAO, Shan MENG, Jinzhong ZHANG, Wenhua FENG, Shuo DONG, Jianping CHEN, Yanbao ZHAO, Laigui YU, Rongrong YING, Xueyan ZOU. Dual‐surface capped hydroxyapatite nano‐amendment with tuned alternate long‐short chain configuration for efficient adsorption towards multi‐heavy metal ions in complex‐contaminated systems[J]. Chinese Journal of Inorganic Chemistry, ;2025, 41(7): 1427-1438. doi: 10.11862/CJIC.20240431 shu

Dual‐surface capped hydroxyapatite nano‐amendment with tuned alternate long‐short chain configuration for efficient adsorption towards multi‐heavy metal ions in complex‐contaminated systems

Mochou GAO ^{1, 2, 3} ,
Shan MENG ^{2, 4} ,
Jinzhong ZHANG ⁵ ,
Wenhua FENG ^{1, 2} ,
Shuo DONG ⁶ ,
Jianping CHEN ^{1, 2} ,
Yanbao ZHAO ^{1, 2} ,
Laigui YU ² ,
Rongrong YING ^1,, ,
Xueyan ZOU ^{1, 2,,}

1.
State Environmental Protection Key Laboratory of Soil Environmental Management and Pollution Control, Nanjing Institute of Environmental Sciences, Ministry of Ecology and Environment of China, Nanjing 210042, China
2.
Institute of Nanoscience and Engineering, Henan University, Zhengzhou 450046, China
3.
State Key Laboratory of Inorganic Synthesis and Preparative Chemistry-College of Chemistry, Jilin University, Changchun 130012, China
4.
College of Chemistry and Molecular Sciences, Henan University, Zhengzhou 450046, China
5.
Department of Chemistry and Biochemistry, University of California, Santa Cruz, California 90095, USA
6.
School of Basic Medical Sciences, Henan University, Zhengzhou 450046, China

Corresponding author: Rongrong YING, yrr@nies.org Xueyan ZOU, zouxueyan@henu.edu.cn
Received Date: 6 December 2024
Revised Date: 9 May 2025

Figures(9)

Hydroxyapatite nanoparticles (HAP NPs) were synthesized by a one‐step hydrothermal method. The surface of HAP NPs was grafted —SH and —COOH chelating groups via in situ surface‐modification with iminodiacetic acid (IDA) and 3‐mercaptopropyl trimethoxysilane (MPS) to afford dual surface‐capped nano‐amendment HAP‐IDA/MPS. The structure of HAP‐IDA/MPS was characterized, and its adsorption performance for Hg²⁺, Cu²⁺, Zn²⁺, Ni²⁺, Co²⁺, and Cd²⁺ was evaluated. The total adsorption capacity of 0.10 g HAP‐IDA/MPS nano‐amendment for Hg²⁺, Cu²⁺, Zn²⁺, Ni²⁺, Co²⁺, and Cd²⁺ with an initial mass concentration of 20 mg·L^-1 reached 13.7 mg·g^-1, about 4.3 times as much as that of HAP. Notably, HAP‐IDA/MPS nano‐amendment displayed the highest immobilization rate for Hg²⁺, possibly because of its chemical reaction with —SH to form sulfide, possessing the lowest solubility product constant among a variety of metal sulfides.
- heavy metal,
- hydroxyapatite,
- nano‐amendment,
- configuration tuning,
- synergistic adsorption
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