Citation: Lin-Yu MEI, Sha LI, Yun-Peng SHAO, Cong-Yun ZHANG, Jun-Yuan WANG. Controlled Fabrication and Surface Enhanced Raman Scattering Performance of Flower-like Silver with Assistance of Citric Acid[J]. Chinese Journal of Inorganic Chemistry, ;2021, 37(7): 1295-1300. doi: 10.11862/CJIC.2021.140 shu

Controlled Fabrication and Surface Enhanced Raman Scattering Performance of Flower-like Silver with Assistance of Citric Acid

1.
School of Mechanical Engineering, North University of China, Taiyuan 030051, China
2.
School of Materials Science and Engineering, North University of China, Taiyuan 030051, China

Corresponding author: Jun-Yuan WANG, wjy@nuc.edu.cn
Received Date: 8 January 2021
Revised Date: 8 April 2021

Figures(5)

Flower-like silver particles with tunable size and shape had been synthesized in one-step by reducing silver nitrate (AgNO₃) with ascorbic acid as reducing agent and citric acid as structure directing agent. The size of nanoparticles could be adjusted from 600 to 1 200 nm, and the surface protrusion could reach 10~25 nm. The chemical nature of citric acid played a vital role in the process of assembling silver nanoparticles into flower-like hierarchical structure. The anisotropic morphologies of as-synthesized silver structures could be readily tuned by varying the dosage of citric acid or ascorbic acid solution. The textured flower-like Ag particles were tested as substrates for the surface enhanced Raman scattering (SERS) and showed high sensitivity for detecting rhodamine 6G (R6G) at a concentration as low as 10^-10 mol·L^-1.
- citric acid,
- flower-like silver structure,
- crystal growth,
- surface enhanced Raman scattering
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沈阳化工大学材料科学与工程学院沈阳 110142