Citation: LI Zhi-Xue, REN Tie-Qiang, GENG Zhong-Xing, YANG Zhan-Xu. Preparation and Electrocatalytic Performance of Flake Co₉S₈/ZnS/C Composites for Oxygen Evolution Reduction[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(12): 2318-2322. doi: 10.11862/CJIC.2019.266 shu

Preparation and Electrocatalytic Performance of Flake Co₉S₈/ZnS/C Composites for Oxygen Evolution Reduction

College of Chemistry, Chemical Engineering and Environmental Engineering, Liaoning Shihua University, Fushun, Liaoning 113006, China

Corresponding author: YANG Zhan-Xu, zhanxuy@126.com
Received Date: 5 July 2019
Revised Date: 29 October 2019

Figures(7)

The flake Co₉S₈/ZnS/C composites were prepared by solvothermal method, through using cobalt hexahydrate[Co(NO₃)₂·6H₂O] as cobalt source, zinc hexahydrate nitrate[Zn(NO₃)₂·6H₂O] as zinc source and 2, 2'-thiodiacetic acid (C₄H₆O₄S) as sulfur source. The flake Co₉S₈/ZnS/C composites structure and morphology were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), N₂ adsorption-desorption test. Meanwhile, the results of electrocatalytic oxygen evolution reaction for the flake Co₉S₈/ZnS/C composite showed that it had high electrocatalytic oxygen production performance, with the initial overpotential of 390 mV and the Tafel slope of 144 mV·dec^-1.
- Co₉S₈/C,
- ZnS,
- transition metal,
- water splitting,
- oxygen evolution reaction,
- solvothermal method
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Preparation and Electrocatalytic Performance of Flake Co₉S₈/ZnS/C Composites for Oxygen Evolution Reduction