Citation: SU Bi-Tao, HE Fang-Zhen, DONG Na, XIN Jun-Lian, DONG Yong-Yong, JIN Zheng-Juan. One-Step Synthesis of NiFe₂O₄ Magnetic Nanomaterial via Solvothermal Method[J]. Chinese Journal of Inorganic Chemistry, ;2016, 32(1): 69-73. doi: 10.11862/CJIC.2016.001 shu

One-Step Synthesis of NiFe₂O₄ Magnetic Nanomaterial via Solvothermal Method

Key Laboratory of Eco-Environment-Related Polymer Materials, Ministry of Education of China, Key Laboratory of Polymer Materials of Gansu Province, College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070, China

Corresponding author: SU Bi-Tao, subt0608@163.com
Received Date: 8 July 2015
Revised Date: 15 October 2015

Figures(7)

Through optimizing the experimental conditions (including solvent, solvothermal reaction temperature and time), NiFe₂O₄ magnetic nanomaterial with good crystallization and super paramagnetic performance, was prepared by one-step solvothermal method using Fe (NO₃)₃·9H₂O and Ni (NO₃)₂·6H₂O as raw materials and EtOH as solvent without adding any alkaline precipitation agent or high-temperature crystallization process. The results show that the solvents, H₂O and (H₂O+EtOH), are disadvantageous to the target magnetic species NiFe₂O₄.Under the condition of EtOH as solvent, the proper solvothermal temperature and reaction time must be guaranteed in order to obtain NiFe₂O₄ magnetic nanomaterial with high purity. The magnetic properties of prepared materials are related to the content of NiFe₂O₄ and its crystallization degree. The prominent advantages of this preparation method are of simpleness, speediness, low cost, free pollution from the source and friendly-environment. And the prepared materials have excellent magnetic performance.
- NiFe₂O₄,
- magnetic nanomaterial,
- green synthesis of solvothermal method,
- characterization,
- magnetic property
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One-Step Synthesis of NiFe₂O₄ Magnetic Nanomaterial via Solvothermal Method