Citation: LONG Li-Xia, DU Hui-Ling, AN Qun-Li, SHI Xiang, CHEN Jian. Synthesis and Gas Adsorption Properties of Zeolite A Membrane on Lead Free Piezoelectric Ceramics[J]. Chinese Journal of Inorganic Chemistry, ;2015, (3): 529-535. doi: 10.11862/CJIC.2015.087 shu

Synthesis and Gas Adsorption Properties of Zeolite A Membrane on Lead Free Piezoelectric Ceramics

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College of Materials Science and Engineering, Xian University of Science and Technology, Xian 710054, China

Corresponding author: DU Hui-Ling,
Received Date: 30 September 2014
Available Online: 18 December 2014
Fund Project: 教育部新世纪优秀人才计划(No.NCET-11-1044) (No.NCET-11-1044)国家自然科学基金(No.51372197) (No.51372197)陕西省重点科技创新团队(No. 2014KCT-04)项目资助。 (No. 2014KCT-04)

Zeolite A membranes were synthesized on 0.8Na_0.5Bi_0.5TiO₃-0.2K_0.5Bi_0.5TiO₃ lead free piezoelectric ceramics surface via hydro-thermal synthesis in micro-emulsion solution and clear solution. The zeolite seeds were connected with ceramics surfaces modified by chemical method. The synthesized zeolites and membranes were characterized using XRD, SEM and FTIR. The amount of methane adsorption were measured by piezoelectric resonator method. The results show the A-type zeolite single phase is obtained both by micro-emulsion solution and clear solution. The first coating times of them are designed as 6 and 9 h separately, and the thickness and morphology of zeolite membranes are changed with different coating times. The sensitivity of piezoelectric vibrator can be achieved to 59 Hz/1%CH₄ and 68 Hz/1%CH₄ using zeolite A membranes obtained by micro-emulsion solution and clear solution as adsorption layer.
- zeolite seeds;A-type zeolite membrane;lead-free piezoelectric ceramics;methane adsorption
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沈阳化工大学材料科学与工程学院沈阳 110142