Citation: ZHENG Long-Zhen, KANG Xiao-Wei, JI Yi, ZOU Zhi-Jun, WANG Yi-Min, CHEN Ji-Fang. Preparation of Ag/ZIF-90 Self-Assembled Membrane and Its High SERS Performance[J]. Chinese Journal of Inorganic Chemistry, ;2015, (3): 465-471. doi: 10.11862/CJIC.2015.079 shu

Preparation of Ag/ZIF-90 Self-Assembled Membrane and Its High SERS Performance

1.
School of Sciences, East China Jiao Tong University, Nanchang 330013, China

Corresponding author: ZHENG Long-Zhen,
Received Date: 16 August 2014
Available Online: 7 November 2014
Fund Project: 国家自然科学基金(No.21163007, 21165009, 21465011) (No.21163007, 21165009, 21465011) 江西省主要学科学术和技术带头人计划(No.20133BCB22007) (No.20133BCB22007)江西省自然科学基金(No.20132BAB203012)资助项目。 (No.20132BAB203012)

Zeolitic imidazolate framework-90 (ZIF-90) sol-gel and ZIF-90 crystal membrane were prepared. Then silver nanoparticles(Ag NPs) were hosted in the ZIF-90 sol-gel or on the ZIF-90 crystal membrane to form Ag@ZIF-90 composite or Ag/ZIF-90 self-assembled membrane. The Ag@ZIF-90 composite and Ag/ZIF-90 self-assembled membrane were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and scanning electron microscopy (SEM) to show their morphorogies and structural features. Rhodamine 6G (R 6G) was used as a detection molecule to test the surface enhanced Raman scattering (SERS) performance of Ag@ZIF-90 composite and Ag/ZIF-90 self-assembled membrane. The SERS signal of R 6G on Ag/ZIF-90 self-assembled membrane was much higher than that on Ag@ZIF-90 composite and the background peak of ZIF-90 did not affect the SERS detection. The Ag/ZIF-90 self-assembled membrane was a promising active SERS substrate, which can be applied in the trace detection of pesticide residue.
- zeolitic imidazolate frameworks;Ag@ZIF-90 composite;Ag/ZIF-90 self-assembled membrane; surface enhanced Raman scattering (SERS)
1. [1]
  [1] Silva C, Corma A, García H. J. Mater. Chem., 2010,20:3141 -3156
2. [2]
  [2] Kreno L, Leong K, Farha O, et al. Chem. Rev., 2011,112: 1105-1125
3. [3]
  [3] Bétard A, Fischer R. Chem. Rev., 2011,112:1055-1083
4. [4]
  [4] Guo H, Zhu G, Hewitt I, et al. J. Am. Chem. Soc., 2009,131: 1646-1647
5. [5]
  [5] Nan J, Dong X, Wang W, et al. Langmuir, 2011,27:4309-4312
6. [6]
  [6] Yoo Y, Varela-Guerrero V, Jeong H. Langmuir, 2011,27: 2652-2657
7. [7]
  [7] Yao J, Dong D, Li D, et al. Chem. Commun., 2011,47:2559-2561
8. [8]
  [8] Park K S, Ni Z, Cté A, et al. Proc. Natl. Acad. Sci. U.S.A., 2006,103:10186-10191
9. [9]
  [9] Banerjee R, Phan A, Wang B, et al. Science, 2008,319:939-943
10. [10]
  [10] Phan A, Doonan C, Uribe-Romo F, et al. Acc. Chem. Res., 2010,43:58-67
11. [11]
  [11] Li Y, Liang F, Bux H, et al. Angew. Chem. Int. Ed., 2010, 122:558-561
12. [12]
  [12] Shekhah O, Eddaoudi M. Chem. Commun., 2013,49:10079-10081
13. [13]
  [13] Huang A, Bux H, Steinbach F, et al. Angew. Chem. Int. Ed., 2010,122:5078-5081
14. [14]
  [14] Hou X, Li H. J. Phys. Chem. C, 2010,114:13501-13508
15. [15]
  [15] Liu Y, Hu E, Khan E, et al. J. Membr. Sci., 2010,353:36-40
16. [16]
  [16] Bae T, Lee J, Qiu W, et al. Angew. Chem. Int. Ed., 2010, 49:9863-9866
17. [17]
  [17] Huang A, Dou W, Caro J. J. Am. Chem. Soc., 2010,132: 15562-15564
18. [18]
  [18] Huang A, Wang N, Kong C, et al. Angew. Chem. Int. Ed., 2012,51:10551-10555
19. [19]
  [19] Esken D, Turner S, Lebedev O, et al. Chem. Mater., 2010, 22:6393-6401
20. [20]
  [20] Kontos A, Likodimos V, Veziri C, et al. ChemSusChem, 2014,7:1696-1702
21. [21]
  [21] HUANG Qing-Li(黄庆利), ZHU Xia-Shi(朱霞石). Chinese J. Inorg. Chem.(无机化学学报), 2014,30(2):442-450
22. [22]
  [22] MENG Wei(孟卫), ZHANG Ling-Yan(张玲艳), JIANG Xiao-Hong(江晓红), et al. Chinese J. Inorg. Chem.(无机化学学报), 2013,29(3):571-576
23. [23]
  [23] XIAO Gui-Na(肖桂娜), MAN Shi-Qing(满石清), LIU Ying-Liang(刘应亮), et al. Chinese J. Inorg. Chem.(无机化学学报), 2007,23(10):1738-1742
24. [24]
  [24] Ikeda K, Suzuki S, Uosaki K. J. Am. Chem. Soc., 2013,135: 17387-17392
25. [25]
  [25] Driskell J, Shanmukh S, Liu Y, et al. J. Phys. Chem. C, 2008,112:895-901
26. [26]
  [26] Sun Y, Xia Y. Nano Lett., 2003,3:675-679
27. [27]
  [27] Siekkinen A, McLellan J, Chen J, et al. Chem. Phys. Lett., 2006,432:491-496
28. [28]
  [28] Rycenga M, Langille M, Personick M, et al. Nano Lett., 2012,12:6218-6222
1. [1]
  Liang MA , Honghua ZHANG , Weilu ZHENG , Aoqi YOU , Zhiyong OUYANG , Junjiang CAO . Construction of highly ordered ZIF-8/Au nanocomposite structure arrays and application of surface-enhanced Raman spectroscopy. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1743-1754. doi: 10.11862/CJIC.20240075
2. [2]
  Meng Lin , Hanrui Chen , Congcong Xu . Preparation and Study of Photo-Enhanced Electrocatalytic Oxygen Evolution Performance of ZIF-67/Copper(I) Oxide Composite: A Recommended Comprehensive Physical Chemistry Experiment. University Chemistry, 2024, 39(4): 163-168. doi: 10.3866/PKU.DXHX202308117
3. [3]
  Min LI , Xianfeng MENG . Preparation and microwave absorption properties of ZIF-67 derived Co@C/MoS₂ nanocomposites. Chinese Journal of Inorganic Chemistry, 2024, 40(10): 1932-1942. doi: 10.11862/CJIC.20240065
4. [4]
  Chen LU , Qinlong HONG , Haixia ZHANG , Jian ZHANG . Syntheses, structures, and properties of copper-iodine cluster-based boron imidazolate framework materials. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 149-154. doi: 10.11862/CJIC.20240407
5. [5]
  Zhuomin Zhang , Hanbing Huang , Liangqiu Lin , Jingsong Liu , Gongke Li . Course Construction of Instrumental Analysis Experiment: Surface-Enhanced Raman Spectroscopy for Rapid Detection of Edible Pigments. University Chemistry, 2024, 39(2): 133-139. doi: 10.3866/PKU.DXHX202308034
6. [6]
  Peng XU , Shasha WANG , Nannan CHEN , Ao WANG , Dongmei YU . Preparation of three-layer magnetic composite Fe₃O₄@polyacrylic acid@ZiF-8 for efficient removal of malachite green in water. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 544-554. doi: 10.11862/CJIC.20230239
7. [7]
  Wei Peng , Baoying Wen , Huamin Li , Yiru Wang , Jianfeng Li . Exploration and Practice on Raman Scattering Spectroscopy Experimental Teaching. University Chemistry, 2024, 39(8): 230-240. doi: 10.3866/PKU.DXHX202312062
8. [8]
  Xin Zhou , Zhi Zhang , Yun Yang , Shuijin Yang . A Study on the Enhancement of Photocatalytic Performance in C/Bi/Bi₂MoO₆ Composites by Ferroelectric Polarization: A Recommended Comprehensive Chemical Experiment. University Chemistry, 2024, 39(4): 296-304. doi: 10.3866/PKU.DXHX202310008
9. [9]
  Guangming YIN , Huaiyao WANG , Jianhua ZHENG , Xinyue DONG , Jian LI , Yi'nan SUN , Yiming GAO , Bingbing WANG . Preparation and photocatalytic degradation performance of Ag/protonated g-C₃N₄ nanorod materials. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1491-1500. doi: 10.11862/CJIC.20240086
10. [10]
  Yihan Xue , Xue Han , Jie Zhang , Xiaoru Wen . NCQDs修饰FeOOH基复合材料的制备及其电容脱盐性能. Acta Physico-Chimica Sinica, 2025, 41(7): 100072-. doi: 10.1016/j.actphy.2025.100072
11. [11]
  Kexin Dong , Chuqi Shen , Ruyu Yan , Yanping Liu , Chunqiang Zhuang , Shijie Li . Integration of Plasmonic Effect and S-Scheme Heterojunction into Ag/Ag₃PO₄/C₃N₅ Photocatalyst for Boosted Photocatalytic Levofloxacin Degradation. Acta Physico-Chimica Sinica, 2024, 40(10): 2310013-. doi: 10.3866/PKU.WHXB202310013
12. [12]
  Qiuting Zhang , Fan Wu , Jin Liu , Zian Lin . Chromatographic Stationary Phase and Chiral Separation Using Frame Materials. University Chemistry, 2025, 40(4): 291-298. doi: 10.12461/PKU.DXHX202405174
13. [13]
  Guang Huang , Lei Li , Dingyi Zhang , Xingze Wang , Yugai Huang , Wenhui Liang , Zhifen Guo , Wenmei Jiao . Cobalt’s Valor, Nickel’s Foe: A Comprehensive Chemical Experiment Utilizing a Cobalt-based Imidazolate Framework for Nickel Ion Removal. University Chemistry, 2024, 39(8): 174-183. doi: 10.3866/PKU.DXHX202311051
14. [14]
  Jiahong ZHENG , Jiajun SHEN , Xin BAI . Preparation and electrochemical properties of nickel foam loaded NiMoO₄/NiMoS₄ composites. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 581-590. doi: 10.11862/CJIC.20230253
15. [15]
  Bowen Yang , Rui Wang , Benjian Xin , Lili Liu , Zhiqiang Niu . C-SnO₂/MWCNTs Composite with Stable Conductive Network for Lithium-based Semi-Solid Flow Batteries. Acta Physico-Chimica Sinica, 2025, 41(2): 100015-. doi: 10.3866/PKU.WHXB202310024
16. [16]
  Fangfang WANG , Jiaqi CHEN , Weiyin SUN . CuBi@Cu-MOF composite catalysts for electrocatalytic CO₂ reduction to HCOOH. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 97-104. doi: 10.11862/CJIC.20240350
17. [17]
  Guanghui SUI , Yanyan CHENG . Application of rice husk-based activated carbon-loaded MgO composite for symmetric supercapacitors. Chinese Journal of Inorganic Chemistry, 2025, 41(3): 521-530. doi: 10.11862/CJIC.20240221
18. [18]
  Shihui Shi , Haoyu Li , Shaojie Han , Yifan Yao , Siqi Liu . Regioselectively Synthesis of Halogenated Arenes via Self-Assembly and Synergistic Catalysis Strategy. University Chemistry, 2024, 39(5): 336-344. doi: 10.3866/PKU.DXHX202312002
19. [19]
  Wenjian Zhang , Mengxin Fan , Wenwen Fei , Wei Bai . Cultivation of Critical Thinking Ability: Based on RAFT Polymerization-Induced Self-Assembly. University Chemistry, 2025, 40(4): 108-112. doi: 10.12461/PKU.DXHX202406099
20. [20]
  Jingyi Chen , Fu Liu , Tiejun Zhu , Kui Cheng . Practice of Integrating Ideological and Political Education into Raman Spectroscopy Analysis Experiment Course. University Chemistry, 2024, 39(2): 140-146. doi: 10.3866/PKU.DXHX202310111

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(264)
HTML views(32)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142