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Citation: SUN Li-Ping, LI Qiang, ZHAO Hui, WANG Hai-Long, HUO Li-Hua. Preparation and Electrochemical Properties of La1.6Sr0.4NiO4-Ag Hollow Nanofibers[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(5): 1045-1050. doi: 10.11862/CJIC.2014.049 shu

Preparation and Electrochemical Properties of La1.6Sr0.4NiO4-Ag Hollow Nanofibers

  • 1.

    Key Laboratory of Functional Inorganic Material Chemistry, Ministry of Education, School of Chemistry and Materials Science, Heilongjiang University, Harbin 150080

  • Received Date: 26 June 2013
    Available Online: 11 October 2013

    Fund Project: 国家自然科学基金(No.51302069，51372073)；黑龙江省杰出青年科学基金(JC201211) (No.51302069，51372073)；黑龙江省杰出青年科学基金(JC201211)黑龙江省自然科学基金(B201107)资助项目。 (B201107)

  • La1.6Sr0.4NiO4-Ag hollow nanofibers are successfully prepared by electro-spinning technology. The phase and morphology of the materials are characterized by XRD and SEM. The results show that La1.6Sr0.4NiO4-Ag hollow nanofibers with an average diameter in 400 nm are obtained after sintering at 800 ℃ for 2 h. The La1.6Sr0.4NiO4-Ag nanofiber forms mesh-like morphology and good contact with the electrolyte after sintering at 850 ℃ for 1 h. The Electrochemical Impedance Spectroscopy (EIS) measurements show that the area specific resistance (ASR) of La1.6Sr0.4NiO4-Ag nanofiber cathode is 0.32 cm2 at 700 ℃ in air. The oxygen partial pressure measurement indicates that the rate limiting step of the nanofiber cathode is charge transfer process from 600 to 700 ℃.
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