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Citation: Ze-ping Zhang, Min-zhi Rong, Ming-qiu Zhang. Research Progress of Processing of Crosslinked Polymers Based on Reversible Covalent Chemistry: a New Challenge to the Development of Polymer Engineering[J]. Acta Polymerica Sinica, ;2018, 0(7): 829-852. doi: 10.11777/j.issn1000-3304.2018.18060 shu

Research Progress of Processing of Crosslinked Polymers Based on Reversible Covalent Chemistry: a New Challenge to the Development of Polymer Engineering

  • Key Laboratory for Polymeric Composite and Functional Materials of Ministry of Education, School of Chemistry, Sun Yat-sen University, Guangzhou 510275

  • Reversible covalent polymers are able to reorganize their topological structures via reversible reactions triggered by external stimuli (including heating, light and pH), while retaining the stability of irreversible covalent polymers in the absence of the stimuli. Because the transformation only deals with polymerized materials and can be conducted mostly in solid state in the absence of solvents, environmentally friendly and energy saving measures, like self-healing that autonomously repairs damages created during fabrication or usage, have been proposed. In the meantime, many researchers are also devoted to using this feature for solving processing problems of crosslinked polymers. It not only breaks through the strict limits of traditional thermoplastic and thermosetting polymers, but also brings in new methods and new functionalities. As a result, material diversification with extended life cycles becomes available. A series of novel prototype techniques specified for the crosslinked polymers containing reversible covalent bonds are developed accordingly, which include mechanical properties regulation, plastic deformation, welding, dispersion of nano-fillers and their reinforcement effect, compression molding, injection molding, extrusion molding, 3D printing, controllable degradation and reprocessing of carbon fibre reinforced composites. Quite a few engineering processes that cannot be realized by means of existing industrial methods come true. Clearly, the research achievements in this area represent possible advancement of classic polymer engineering. In this review, basis of reversible covalent chemistry and rheology of reversible covalent polymer are comprehensively elucidated and analysed, followed by summarizing the applications of above prototype techniques on the basis of the types of the reversible reactions involved (i.e. general reversible reactions and dynamic reversible reactions). Moreover, the challenges and development trend of this emerging field are also outlined. On the whole, the innovative knowledge paths are managed to be introduced in a systematic way. It is hoped that more and more scientists will be attracted and join in this promising research.
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