Citation: Hui-Xian Jiang, Zhi-Tao Liu, Pei Xu, Xu Zhu. Synthetic application of oxalate salts for visible-light-induced radical transformations[J]. Chinese Chemical Letters, ;2025, 36(12): 111224. doi: 10.1016/j.cclet.2025.111224 shu

Synthetic application of oxalate salts for visible-light-induced radical transformations

Hui-Xian Jiang ¹ ,
Zhi-Tao Liu ¹ ,
Pei Xu ^*, ,
Xu Zhu ^*,

Jiangsu Key Laboratory of New Drug Research and Clinical Pharmacy, School of Pharmacy, Xuzhou Medical University, Xuzhou 221004, China

xupei@xzhmu.edu.cn

xuzhu@xzhmu.edu.cn

Received Date: 3 January 2025
Revised Date: 27 March 2025
Accepted Date: 16 April 2025
Available Online: 16 April 2025

Figures(13)

Oxalic acid salts (oxalate) were recently developed as C1 synthon, potent single-electron-transfer (SET) reductant, and hole scavengers via generation of CO₂ and CO₂ radical anion (CO₂^•−) under mild photochemical conditions. A series of challenging reductive transformations were realized with oxalic dianion under catalytic photoredox conditions or through an electron-donor-acceptor (EDA) complex formation process. As a chemical intermediate for carbon capture and utilization (also a cheap and readily available reagent), oxalate salts could release one electron easily (E_ox = +0.06 V vs. SCE) via visible-light irradiation to give CO₂ and CO₂^•− and therefore opened a new arena for reductive carboxylation reactions with highly expanded reaction diversity and chemical space to realize challenging C-X bond activation, alkenes cross coupling, and reductive carboxylation of unsaturated chemical bonds in a more sustainable and efficient way. This review features the recently developed aspects with oxalate salts and also an outlook for its further application in organic radical transformations.
- Oxalate salts,
- CO₂ radical anion,
- CO₂ capture,
- Photocatalysis,
- Radical carboxylation,
- EDA complex
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