Citation: Ming-Yu Li, Shi-Chao Cheng, Dan Li, Shen-Nan Wang, An-Min Huang, Su-Qin Sun. Structural characterization of steam-heat treated Tectona grandis wood analyzed by FT-IR and 2D-IR correlation spectroscopy[J]. Chinese Chemical Letters, ;2015, 26(2): 221-225. doi: 10.1016/j.cclet.2014.11.024 shu

Structural characterization of steam-heat treated Tectona grandis wood analyzed by FT-IR and 2D-IR correlation spectroscopy

  • Corresponding author: An-Min Huang, 
  • Received Date: 3 September 2014
    Available Online: 13 November 2014

    Fund Project: This work was sponsored by the National Natural Science Foundation of China (No. 31270591) (No. 31270591)

  • The properties of wood can be improved through steam-heat treatment. There are many studies about mechanical properties of steam-heat treated wood, but very few studies are on the aspects of chemical modifications. In this study, FT-IR spectra combined with SD-IR spectra, correlation coefficients and 2DIR spectra are employed to analyze the chemicalmodifications of teak (Tectona grandis L.F.) wood during steam-heat treatment under treatment temperatures from 120℃ to 220℃ at intervals of 20℃. Acetic acid, which is produced during steam-heat treatment, acts as a catalyst of condensation and degradation reactions of wood components. The changes of wood components are more and more intense with increasing the treatment temperature. The sensitivity of wood samples to thermal perturbation rises initially with increasing treatment temperature before falling back. The steam-heat treated wood under 180℃ is the most sensitive.
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    1. [1]

      [1] C.-M. Popescu, M.-C. Popescu, A near infrared spectroscopic study of the structural modifications of lime (Tilia cordata Mill.) wood during hydro-thermal treatment, Spectrochim. Acta A: Mol. Biomol. Spectrosc. 115 (2013) 227-233.

    2. [2]

      [2] P. Navi, D. Sandberg, Thermo-hydro-mechanical Wood Processing, CRC Press, Boca Raton, 2012.

    3. [3]

      [3] B.M. Esteves, H.M. Pereira, Wood modification by heat treatment: a review, Bioresources 4 (2009) 370-404.

    4. [4]

      [4] B. Esteves, J. Graca, H. Pereira, Extractive composition and summative chemical analysis of thermally treated eucalypt wood, Holzforschung 62 (2008) 344-351.

    5. [5]

      [5] Y.J. Cao, J.X. Lu, R.F. Huang, X. Zhao, J.L. Jiang, Effect of steam-heat treatment on mechanical properties of Chinese fir, Bioresources 7 (2012) 1123-1133.

    6. [6]

      [6] B. Esteves, R. Videira, H. Pereira, Chemistry and ecotoxicity of heat-treated pine wood extractives, Wood Sci. Technol. 45 (2011) 661-676.

    7. [7]

      [7] M.-C. Popescu, J. Froidevaux, P. Navi, C.-M. Popescu, Structural modifications of Tilia cordata wood during heat treatment investigated by FT-IR and 2D IR correlation spectroscopy, J. Mol. Struct. 1033 (2013) 176-186.

    8. [8]

      [8] S.Q. Sun, Q. Zhou, J.B. Chen, Infrared Spectroscopy for Complex Mixtures-Applications in Food and Traditional Chinese Medicine, Chemical Industry Press, Beijing, 2011.

    9. [9]

      [9] Z. Yang, H. Lin, T. Gui, R.F. Zhou, X.S. Chen, Infrared spectroscopy of N-methylacetamide in water from high-level QM/MM calculations, Chin. Chem. Lett. 25 (2014) 107-110.

    10. [10]

      [10] X.Q. Lin, Z.X. Zhang, W.Q. Hu, Concave cell design for FTIR measurements, Chin. Chem. Lett. 22 (2011) 1339-1342.

    11. [11]

      [11] C.-M. Popescu, B.C. Simionescu, Structural study of photodegraded acrylic-coated lime wood using Fourier transform infrared and two-dimensional infrared correlation spectroscopy, Appl. Spectrosc. 67 (2013) 606-613.

    12. [12]

      [12] C.-M. Popescu, M.-C. Popescu, C. Vasile, Structural changes in biodegraded lime wood, Carbohydr. Polym. 79 (2010) 362-372.

    13. [13]

      [13] H.L. Liu, J. Shang, X.Q. Chen, F.A. Kamke, K.Q. Guo, The influence of thermal-hydromechanical processing on chemical characterization of Tsuga heterophylla, Wood Sci. Technol. 48 (2014) 373-392.

    14. [14]

      [14] I. Noda, Two-dimensional infrared (2-D IR) spectroscopy of synthetic and biopolymers, Bull. Am. Phys. Soc. 31 (1986) 520.

    15. [15]

      [15] Q. Zhou, J.B. Chen, S.Q. Sun, What can two-dimensional correlation infrared spectroscopy (2D-IR) tell us about the composition, origin and authenticity of herbal medicines, Biomed. Spectrosc. Imaging 2 (2013) 101-113.

    16. [16]

      [16] A.M. Huang, Q. Zhou, J.L. Liu, B.H. Fei, S.Q. Sun, Distinction of three wood species by Fourier transform infrared spectroscopy and two-dimensional correlation IR spectroscopy, J. Mol. Struct. 833-834 (2008) 160-166.

    17. [17]

      [17] C.-M. Popescu, M.-C. Popescu, C. Vasile, Structural analysis of photodegraded lime wood by means of FT-IR and 2D IR correlation spectroscopy, Int. J. Biol. Macromol. 48 (2011) 667-675.

    18. [18]

      [18] C.-M. Popescu, M.-C. Popescu, C. Vasile, Characterization of fungal degraded lime wood by FT-IR and 2D IR correlation spectroscopy, Microchem. J. 95 (2010) 377-387.

    19. [19]

      [19] T. Kondo, Polysaccharides II—structural diversity and functional versatility, in: S. Dumitriu (Ed.), Hydrogen Bonds in Cellulose and Cellulose Derivatives, Marcel Dekker, New York, 2005 (Chapter 3).

    20. [20]

      [20] S. Kubo, J.F. Kadla, Hydrogen bonding in lignin: a Fourier transform infrared model compound study, Biomacromolecules 6 (2005) 2815-2821.

    21. [21]

      [21] E. Windeisen, G. Wegener, Behaviour of lignin during thermal treatments of wood, Ind. Crop Prod. 27 (2008) 157-162.

    22. [22]

      [22] Y. Chen, Y. Fan, J. Gao, N.M. Stark, The effect of heat treatment on the chemical and color change of black locust (Robinia pseudoacacia) wood flour, Bioresources 7 (2012) 1157-1170.

    23. [23]

      [23] O. Faix, Fourier Transform Infrared Spectroscopy, Methods in Lignin Chemistry, Springer, Berlin/Heidelberg, 1992, pp. 83-109.

    24. [24]

      [24] O. Faix, J.H. Bö ttcher, The influence of particle size and concentration in transmission and diffuse reflectance spectroscopy of wood, Eur. J. Wood Wood Prod. 50 (1992) 221-226.

    25. [25]

      [25] M.M. Gonzá lez-Penã, M.D.C. Hale, Rapid assessment of physical properties and chemical composition of thermally modified wood by mid-infrared spectroscopy, Wood Sci. Technol. 45 (2011) 83-102.

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