Citation:
Xiang Qin Lin, Zhi Xiang Zhang, Wan Qun Hu. A V-shaped spectroscopic cell for FTIR measurements[J]. Chinese Chemical Letters,
;2011, 22(4): 481-484.
doi:
10.1016/j.cclet.2010.10.043
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A V-shaped spacroscopic cell (V-cell) was constructed using two CaF2 optical plates for FTIR light transparent measurements in the range of 4000-1000 cm-1. The spectrum of ethanol was characterized with the standard spectra, excellent fitting was achieved with a bottom-width correction method. The principle of the V-cell was discussed, giving equations for the data interpretation. It shows that the V-cell is an auto-focus type spectroscopic cell, which can effectively avoid absorption saturation with amplifications for weak absorption bands. The V-cell design is simple and effective, easy to operate, suitable for applications in liquid samples with high absorption bands, willing to have broad application prospects.
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