Citation: Liang Chun Wu, Long Qing Liu, Hai Shan Jin, Ming Liang Ma, Xiao Li Zhao, Ke Wen. Synthesis and structure determination of pyrazine-containing macrocyclic polyazomethines[J]. Chinese Chemical Letters, ;2010, 21(10): 1263-1266. doi: 10.1016/j.cclet.2010.05.017 shu

Synthesis and structure determination of pyrazine-containing macrocyclic polyazomethines

a Division of Supramolecular Chemistry and Medicinal Chemistry, Key Laboratory of Brain Functional Genomics, MOE, and Shanghai Key Laboratory of Brain Functional Genomics, East China Normal University, Shanghai 200062, China;
b Shanghai Key Laboratory of Green Chemistry and Chemical Processes, and Department of Chemistry, East China Normal University, Shanghai 200062, China

Received Date: 4 March 2010

Fund Project: The authors thank Shanghai Commission for Science and Technology (Nos.06Pj14034,06DZ19002,and 10ZR1409700),Ministry of Education (No.106078) for financial support.

Two pyrazine-containing macrocyclic polyazomethines 2 and 3 were synthesized by direct[2+2]and[3+3]condensation reactions between 2, 2'-[pyrazine-2, 3-diylbis(oxy)]dibenzaldehyde (1) and hydrazine. Both 2 and 3 were characterized by NMR, HRMS, and their structures were determined via X-ray crystal diffraction studies.
- Azomethine,
- Macrocycles,
- Schiff base,
- Pyrazine
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