Citation: Rui Feng Wu, Tong Lai Zhang, Xiao Jing Qiao. Synthesis and characterization of an intermediary of new heat-resistant energetic materials[J]. Chinese Chemical Letters, ;2010, 21(8): 1007-1010. doi: 10.1016/j.cclet.2010.02.006 shu

Synthesis and characterization of an intermediary of new heat-resistant energetic materials

a College of Chemical Engineering, Inner Mongolia University of Technology, Hohhot 010051, China;
b State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081, China

Received Date: 3 November 2009

Fund Project: This paper is supported by the opening project of State Key Laboratory of Explosion Science and Technology (Beijing Institute of Technology, No. KFJJ10-7M), Key Project of Inner Mongolia University of Technology (No. ZD200806).

Nitration of 4,4'-biphenyldicarboxylic acid (BPDC) was studied and an aromatic carboxylic acid containing two nitro groups was synthesized and characterized through elemental analysis and IR spectra. Crystal structure of DNBPDC (DNBPDC=2,2'-dinitro-4,4'-biphenyldicarboxylic acid) was determined by X-ray single crystal diffraction and the thermal decomposition was carried out through DSC and TG-DTG analyses.
- Energetic material,
- Thermal analysis,
- Crystal structure
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