Citation: Juan Juan Ren, Hai Yan Liu, Yu Hong Hao, Pin Gang He, Yu Zhi Fang. Determination of resveratrol in red wine by solid phase extraction-flow injection chemiluminescence method[J]. Chinese Chemical Letters, ;2007, 18(8): 985-988. doi: 10.1016/j.cclet.2007.06.013 shu

Determination of resveratrol in red wine by solid phase extraction-flow injection chemiluminescence method

a Department of Chemistry, East China Normal University, Shanghai 200062, China;
b School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai 200237, China

Received Date: 10 April 2007

A sensitive flow injection chemiluminescence method has been developed for the detection of resveratrol in red wine based on the fact that resveratrol can greatly enhance chemiluminescence reaction between KMnO₄ and HCHO in sulfuric acid medium.Analytes were pre-concentrated on solid sorbents (C₁₈ solid-phase extraction cartridges). Under the optimum conditions, the proposed method allows the measurement of resveratrol over the range of 1.32×10^-8 to 1.32×10^-5 mol/L with a detection limit of 3.30×10^-9 mol/L, and the relative standard deviation for 1.32×10^-5mol/L resveratrol (n=11) is 3.8%. This method has been successfully applied for the determination of the resveratrol in red wine. Furthermore, the possible reaction mechanism was also discussed.
- Resveratrol,
- Solid phase extraction,
- Flow-injection chemiluminescence,
- Potassium permanganate,
- Formaldehyde
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