Citation: Bing Zhao, Ya Qing Feng, Yu Kun Li. Synthesis and characterization of a novel series of pyrimidinylthiaalkoxycalix[4]arenes[J]. Chinese Chemical Letters, ;2007, 18(4): 403-406. doi: 10.1016/j.cclet.2007.02.007 shu

Synthesis and characterization of a novel series of pyrimidinylthiaalkoxycalix[4]arenes

School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China

Received Date: 17 November 2006

Fund Project: Thanks for the support of the National Natural Science Foundation of China (No. 20376059).

A novel series of pyrimidinylthiaalkoxycalix[4]arenes with the reaction between 4,6-dimethylpyrimidine-2-thiol and the different dibromides calix[4]aryl groups have been synthesized and structurally characterized by IR, ¹H NMR and MS. From their analysis data, it was found that compounds 8, 9, 11 adopted a cone conformation, while compound 10 existed as a mixture of conformations.
- Pyrimidinylthiaalkoxycalix[4]arenes,
- Synthesis,
- Characterization,
- Conformation
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