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Citation:
Zhi Hao Shi, Yun Yang Wei. Novel synthesis of a strained para-cyclophane derivative[J]. Chinese Chemical Letters,
;2007, 18(4): 397-399.
doi:
10.1016/j.cclet.2007.02.006
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A [P. Rajakumar, A.M.A. Rasheed, Tetrahedron 61(22) (2005) 5351] para-cyclophane derivative was synthesized via intramolecular esterification of a dipeptide surrogate containing asparagine to form tetrahydropyrimidinone ring. The structures of the product and intermediates were characterized by 1H NMR, 13C NMR and mass spectrum.
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Keywords:
- Asparagine,
- Cyclization,
- Para-cyclophane
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