界面工程与氧空位协同策略促进Cd<sub>0.5</sub>Zn<sub>0.5</sub>S/BiOBr S型异质结高效光催化去除抗生素

引用本文: 马德运, 梁凤兰, 薛清泉, 刘艳萍, 庄春强, 李世杰. 界面工程与氧空位协同策略促进Cd_0.5Zn_0.5S/BiOBr S型异质结高效光催化去除抗生素[J]. 物理化学学报, 2025, 41(12): 100190. doi: 10.1016/j.actphy.2025.100190 shu

Citation: Deyun Ma, Fenglan Liang, Qingquan Xue, Yanping Liu, Chunqiang Zhuang, Shijie Li. Interfacial engineering of Cd_0.5Zn_0.5S/BiOBr S-scheme heterojunction with oxygen vacancies for effective photocatalytic antibiotic removal[J]. Acta Physico-Chimica Sinica, 2025, 41(12): 100190. doi: 10.1016/j.actphy.2025.100190 shu

界面工程与氧空位协同策略促进Cd_0.5Zn_0.5S/BiOBr S型异质结高效光催化去除抗生素

马德运 ^1, ,
梁凤兰 ^1, ,
薛清泉 ^{2,
,} ,
刘艳萍 ^3, ,
庄春强 ^{4,
,} ,
李世杰 ^{3,5,
,}

1.
肇庆学院食品与制药工程学院, 生命科学学院, 广东肇庆 526061;
2.
浙江省污染暴露与健康干预重点实验室, 浙江树人大学交叉科学研究院, 浙江杭州 310015;
3.
浙江省港口石油化工污染控制重点实验室, 国家海洋设施养殖工程技术研究中心, 浙江海洋大学, 浙江舟山 316022;
4.
北京工业大学先进材料微观结构与性能研究所, 北京 100124;
5.
河南省废弃物资源能源化工程技术研究中心, 河南大学能源科学与技术学院, 河南郑州 450046

通讯作者: 薛清泉, E-mail: qingquanxue@zjsru.edu.cn; 庄春强, E-mail: chunqiang.zhuang@bjut.edu.cn; 李世杰E-mail: lishijie@zjou.edu.cn

基金项目:
浙江省自然科学基金(LY20E080014), 国家自然科学基金(51708504)及河南大学化学学科开放合作基金(DCSHENU2413)资助

摘要: 构建S型异质结光催化剂已成为解决抗生素废水污染，实现其高效修复的重要策略。然而，半导体间界面接触紧密性不足与电荷转移过程难以精确调控等问题，仍然制约其实际应用。本研究通过可控溶剂热合成法构建了分级Cd_0.5Zn_0.5S/BiOBr S型异质结，其中BiOBr微球作为核芯，Cd_0.5Zn_0.5S纳米颗粒锚定在其表面形成共形外壳。这种结构确保了最大界面接触与定向电荷传输，对优化光催化效率至关重要。优化后的异质结展现出卓越的催化性能，其四环素(TC)降解速率常数分别是纯相BiOBr和Cd_0.5Zn_0.5S的3.3倍和1.6倍。这种增强源于S型机制固有的高效电荷分离与保留氧化还原能力的协同作用。此外，本研究阐明了TC降解过程与机制，为开发高性能缺陷型S型异质结用于抗生素废水净化提供了新视角。

关键词:

English

Interfacial engineering of Cd_0.5Zn_0.5S/BiOBr S-scheme heterojunction with oxygen vacancies for effective photocatalytic antibiotic removal

1.
School of Food and Pharmaceutical Engineering, School of Life Sciences, Zhaoqing University, Zhaoqing 526061, Guangdong Province, China;
2.
Key Laboratory of Pollution Exposure and Health Intervention of Zhejiang Province, Interdisciplinary Research Academy (IRA), Zhejiang Shuren University, Hangzhou 310015, Zhejiang Provincne, China;
3.
Zhejiang Key Laboratory of Pollution Control for Port-Petrochemical Industry, National Engineering Research Center for Marine Aquaculture, Zhejiang Ocean University, Zhoushan 316022, Zhejiang Province, China;
4.
Institute of Microstructure and Property of Advanced Materials, Beijing University of Technology, Beijing 100124, China;
5.
Henan Engineering Research Center of Resource & Energy Recovery from Waste, School of Energy Science and Technology, Henan University, Zhengzhou 450046, Henan Province, China

Corresponding author: Qingquan Xue, ; Chunqiang Zhuang, ; Shijie Li,

Received Date: 10 August 2025
Revised Date: 19 September 2025
Available Online: 19 September 2025
Fund Project:
This work has been financially supported by the Natural Science Foundation of Zhejiang Province (LY20E080014), the National Natural Science Foundation of China (51708504), and the Open Cooperation Foundation of the Department of Chemical Science of Henan University (DCSHENU2413).

Abstract: The construction of S-scheme heterojunction photocatalysts has emerged as a promising strategy to address the urgent need for efficient antibiotic wastewater remediation. However, persistent challenges in achieving interfacial intimacy and precise charge transfer regulation between semiconductors have hindered their practical implementation. In this work, we engineered a hierarchical Cd_0.5Zn_0.5S/BiOBr S-scheme heterojunction via a controlled solvothermal synthesis, where BiOBr microspheres serve as the core, and Cd_0.5Zn_0.5S nanoparticles form a conformal shell. This architecture ensures maximal interfacial contact and directional charge dynamics, critical for optimizing photocatalytic efficiency. The optimized heterojunction exhibits superior catalytic performance, achieving tetracycline (TC) degradation rate constants 3.3- and 1.6-fold greater than pristine BiOBr and Cd_0.5Zn_0.5S, respectively. This enhancement stems from the synergistic interplay of efficient charge separation and preserved redox capacities inherent to the S-scheme mechanism. Furthermore, the TC degradation process and mechanism were elucidated. This study provides a new perspective on developing defective S-scheme heterojunctions for antibiotic wastewater purification with high performance.

Key words:

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沈阳化工大学材料科学与工程学院沈阳 110142

界面工程与氧空位协同策略促进Cd_0.5Zn_0.5S/BiOBr S型异质结高效光催化去除抗生素

通讯作者: 薛清泉, E-mail: qingquanxue@zjsru.edu.cn; 庄春强, E-mail: chunqiang.zhuang@bjut.edu.cn; 李世杰E-mail: lishijie@zjou.edu.cn

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Interfacial engineering of Cd_0.5Zn_0.5S/BiOBr S-scheme heterojunction with oxygen vacancies for effective photocatalytic antibiotic removal

Corresponding author: Qingquan Xue, ; Chunqiang Zhuang, ; Shijie Li,

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界面工程与氧空位协同策略促进Cd0.5Zn0.5S/BiOBr S型异质结高效光催化去除抗生素

通讯作者: 薛清泉, E-mail: qingquanxue@zjsru.edu.cn; 庄春强, E-mail: chunqiang.zhuang@bjut.edu.cn; 李世杰E-mail: lishijie@zjou.edu.cn

English

Interfacial engineering of Cd0.5Zn0.5S/BiOBr S-scheme heterojunction with oxygen vacancies for effective photocatalytic antibiotic removal

Corresponding author: Qingquan Xue, ; Chunqiang Zhuang, ; Shijie Li,

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